(S)-benzyl 3-(3-(benzyloxy)-4-hydroxyphenyl)-2-(((benzyloxy)carbonyl)amino)propanoate

Base Information

Chemical Name:(S)-benzyl 3-(3-(benzyloxy)-4-hydroxyphenyl)-2-(((benzyloxy)carbonyl)amino)propanoate
CAS No.:122769-75-9
Molecular Formula:C₃₁H₂₉NO₆
Molecular Weight:511.574
Hs Code.:

Synonyms:(S)-benzyl 3-(3-(benzyloxy)-4-hydroxyphenyl)-2-(((benzyloxy)carbonyl)amino)propanoate

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Chemical Property of (S)-benzyl 3-(3-(benzyloxy)-4-hydroxyphenyl)-2-(((benzyloxy)carbonyl)amino)propanoate

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Technology Process of (S)-benzyl 3-(3-(benzyloxy)-4-hydroxyphenyl)-2-(((benzyloxy)carbonyl)amino)propanoate

There total 11 articles about (S)-benzyl 3-(3-(benzyloxy)-4-hydroxyphenyl)-2-(((benzyloxy)carbonyl)amino)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 13.6%

: 37169-42-9
(S)-benzyl 2-(((benzyloxy)carbonyl)amino)-3-(3,4-dihydroxyphenyl)propanoate

: 100-44-7
benzyl chloride

: 122769-75-9
(S)-benzyl 3-(3-(benzyloxy)-4-hydroxyphenyl)-2-(((benzyloxy)carbonyl)amino)propanoate

: 122769-76-0
L-N-benzyloxycarbonyl-3-(4-benzyloxy-3-hydroxyphenyl)alanine benzyl ester

Guidance literature:: With potassium carbonate; sodium iodide; In acetone; for 7.5h; Heating;
DOI:10.1002/jps.2600790811

Reference yield:

: 21209-51-8
N-benzyloxycarbonyl-L-serine benzyl ester

: 122769-75-9
(S)-benzyl 3-(3-(benzyloxy)-4-hydroxyphenyl)-2-(((benzyloxy)carbonyl)amino)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: methyltriphenoxyphosphonium iodide / N,N-dimethyl-formamide / 0.33 h / 0 °C

2.1: iodine; zinc / N,N-dimethyl-formamide / 0.33 h / 10 - 25 °C

2.2: 1 h / 20 °C

With methyltriphenoxyphosphonium iodide; iodine; zinc; In N,N-dimethyl-formamide;