N-[2-(2-Benzyloxy-3,4-dimethoxy-phenyl)-ethyl]-2-(3-benzyloxy-4-methoxy-phenyl)-acetamide

Base Information

Chemical Name:N-[2-(2-Benzyloxy-3,4-dimethoxy-phenyl)-ethyl]-2-(3-benzyloxy-4-methoxy-phenyl)-acetamide
CAS No.:35115-16-3
Molecular Formula:C₃₃H₃₅NO₆
Molecular Weight:541.644
Hs Code.:

Synonyms:N-[2-(2-Benzyloxy-3,4-dimethoxy-phenyl)-ethyl]-2-(3-benzyloxy-4-methoxy-phenyl)-acetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[2-(2-Benzyloxy-3,4-dimethoxy-phenyl)-ethyl]-2-(3-benzyloxy-4-methoxy-phenyl)-acetamide

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of N-[2-(2-Benzyloxy-3,4-dimethoxy-phenyl)-ethyl]-2-(3-benzyloxy-4-methoxy-phenyl)-acetamide

There total 10 articles about N-[2-(2-Benzyloxy-3,4-dimethoxy-phenyl)-ethyl]-2-(3-benzyloxy-4-methoxy-phenyl)-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 54313-33-6
2-(3-(benzyloxy)-4-methoxyphenyl)acetyl chloride

: 15778-62-8
2-(2-benzyloxy-3,4-dimethoxyphenyl)ethylamine

: 35115-16-3
N-[2-(2-Benzyloxy-3,4-dimethoxy-phenyl)-ethyl]-2-(3-benzyloxy-4-methoxy-phenyl)-acetamide

Guidance literature:: With sodium carbonate; In dichloromethane; water; at 20 ℃; for 2h;
DOI:10.1021/jo061810h

Reference yield:

: 100-39-0
benzyl bromide

: 35115-16-3
N-[2-(2-Benzyloxy-3,4-dimethoxy-phenyl)-ethyl]-2-(3-benzyloxy-4-methoxy-phenyl)-acetamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / acetone / 6 h / Heating

2.1: acetic acid; ethylenediamine / 20 °C

3.1: sodium tetrahydroborate / ethanol / 20 °C

3.2: AcOH; NaNO₂; DMSO / 20 °C

4.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 2 h / 20 °C

5.1: sodium carbonate / dichloromethane; water / 2 h / 20 °C

With sodium tetrahydroborate; oxalyl dichloride; sodium carbonate; potassium carbonate; acetic acid; ethylenediamine; N,N-dimethyl-formamide; In ethanol; dichloromethane; water; acetone; 2.1: Knoevenagel reaction;
DOI:10.1021/jo061810h

Reference yield:

: 19283-70-6
3,4-dimethoxysalicylaldehyde

: 35115-16-3
N-[2-(2-Benzyloxy-3,4-dimethoxy-phenyl)-ethyl]-2-(3-benzyloxy-4-methoxy-phenyl)-acetamide

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / acetone / 6 h / Heating

2: acetic acid; ethylenediamine / 20 °C

3: lithium aluminium tetrahydride / tetrahydrofuran / 24 h / 20 °C

4: sodium carbonate / dichloromethane; water / 2 h / 20 °C

With lithium aluminium tetrahydride; sodium carbonate; potassium carbonate; acetic acid; ethylenediamine; In tetrahydrofuran; dichloromethane; water; acetone; 2: Knoevenagel reaction;
DOI:10.1021/jo061810h