2-<1-<6-chloro-4-(2-chlorophenyl)-1-phthalazinyl>ethyl>-1H-isoindole-1,3(2H)-dione

Base Information

Chemical Name:2-<1-<6-chloro-4-(2-chlorophenyl)-1-phthalazinyl>ethyl>-1H-isoindole-1,3(2H)-dione
CAS No.:81389-12-0
Molecular Formula:C₂₄H₁₅Cl₂N₃O₂
Molecular Weight:448.308
Hs Code.:

Synonyms:2-<1-<6-chloro-4-(2-chlorophenyl)-1-phthalazinyl>ethyl>-1H-isoindole-1,3(2H)-dione

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Chemical Property of 2-<1-<6-chloro-4-(2-chlorophenyl)-1-phthalazinyl>ethyl>-1H-isoindole-1,3(2H)-dione

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Technology Process of 2-<1-<6-chloro-4-(2-chlorophenyl)-1-phthalazinyl>ethyl>-1H-isoindole-1,3(2H)-dione

There total 4 articles about 2-<1-<6-chloro-4-(2-chlorophenyl)-1-phthalazinyl>ethyl>-1H-isoindole-1,3(2H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 78367-91-6
2-<<4-chloro-2-(2-chlorobenzoyl)phenyl>-3-oxopropyl>-1H-isoindole-1,3(2H)-dione

: 81389-12-0
2-<1-<6-chloro-4-(2-chlorophenyl)-1-phthalazinyl>ethyl>-1H-isoindole-1,3(2H)-dione

Guidance literature:: With hydrazine hydrate; In ethanol; for 2h; steam bath;
DOI:10.1021/jo00133a040

Reference yield:

: 76049-54-2
N-<<4-chloro-2-(2-chlorobenzoyl)phenyl>-3-propynyl>isoindole-1,3(2H)-dione

: 81389-12-0
2-<1-<6-chloro-4-(2-chlorophenyl)-1-phthalazinyl>ethyl>-1H-isoindole-1,3(2H)-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / mercuric sulfate, formic acid / H₂O; CH₂Cl₂ / 0.67 h / Ambient temperature

2: 58 percent / 85percent hydrazine hydrate / ethanol / 2 h / steam bath

With formic acid; hydrazine hydrate; mercury(II) sulfate; In ethanol; dichloromethane; water;
DOI:10.1021/jo00133a040

Reference yield:

: 76049-50-8
2',5-dichloro-2-iodobenzophenone

: 81389-12-0
2-<1-<6-chloro-4-(2-chlorophenyl)-1-phthalazinyl>ethyl>-1H-isoindole-1,3(2H)-dione

Guidance literature:: Multi-step reaction with 3 steps

1: 39 percent / triphenylphosphine, palladium chloride, cuprous iodide, diethylamine / CH₂Cl₂ / 20 h / Ambient temperature

2: 92 percent / mercuric sulfate, formic acid / H₂O; CH₂Cl₂ / 0.67 h / Ambient temperature

3: 58 percent / 85percent hydrazine hydrate / ethanol / 2 h / steam bath

With copper(l) iodide; formic acid; hydrazine hydrate; mercury(II) sulfate; diethylamine; triphenylphosphine; palladium dichloride; In ethanol; dichloromethane; water;
DOI:10.1021/jo00133a040