1-[2-(methylthio)benzoyloxy]-11-iodo-3,6,9-trioxaundecane

Base Information

Chemical Name:1-[2-(methylthio)benzoyloxy]-11-iodo-3,6,9-trioxaundecane
CAS No.:1465846-44-9
Molecular Formula:C₁₆H₂₃IO₅S
Molecular Weight:454.326
Hs Code.:

Synonyms:1-[2-(methylthio)benzoyloxy]-11-iodo-3,6,9-trioxaundecane

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Chemical Property of 1-[2-(methylthio)benzoyloxy]-11-iodo-3,6,9-trioxaundecane

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Technology Process of 1-[2-(methylthio)benzoyloxy]-11-iodo-3,6,9-trioxaundecane

There total 4 articles about 1-[2-(methylthio)benzoyloxy]-11-iodo-3,6,9-trioxaundecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 36839-56-2
1,11-diiodo-3,6-9-trioxaundecane

: 3724-10-5
2-(methylthio)benzoic acid

: 1465846-44-9
1-[2-(methylthio)benzoyloxy]-11-iodo-3,6,9-trioxaundecane

Guidance literature:: With caesium carbonate; In acetone; at 45 ℃; for 24h;
DOI:10.1039/c3cc45305g

Reference yield:

: 147-93-3
Thiosalicylic acid

: 1465846-44-9
1-[2-(methylthio)benzoyloxy]-11-iodo-3,6,9-trioxaundecane

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide / methanol / 0.25 h / Inert atmosphere

1.2: 2 h / 0 °C / Inert atmosphere

2.1: caesium carbonate / acetone / 24 h / 45 °C

With caesium carbonate; sodium hydroxide; In methanol; acetone;
DOI:10.1039/c3cc45305g

Reference yield:

: 112-60-7
Tetraethylene glycol

: 1465846-44-9
1-[2-(methylthio)benzoyloxy]-11-iodo-3,6,9-trioxaundecane

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / 20 °C

2: sodium iodide / acetone / 40 °C

3: caesium carbonate / acetone / 24 h / 45 °C

With caesium carbonate; triethylamine; sodium iodide; In acetone;
DOI:10.1039/c3cc45305g