benzyl 3-<1-(N-methylamino)hexyl>phenyl ether hydrochloride

Base Information

Chemical Name:benzyl 3-<1-(N-methylamino)hexyl>phenyl ether hydrochloride
CAS No.:92532-27-9
Molecular Formula:C₂₀H₂₇NO*ClH
Molecular Weight:333.901
Hs Code.:

Synonyms:benzyl 3-<1-(N-methylamino)hexyl>phenyl ether hydrochloride

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Chemical Property of benzyl 3-<1-(N-methylamino)hexyl>phenyl ether hydrochloride

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Technology Process of benzyl 3-<1-(N-methylamino)hexyl>phenyl ether hydrochloride

There total 6 articles about benzyl 3-<1-(N-methylamino)hexyl>phenyl ether hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 593-51-1
methylamine hydrochloride

: 92532-18-8
benzyl 3-hexanoylphenyl ether

: 92532-27-9
benzyl 3-<1-(N-methylamino)hexyl>phenyl ether hydrochloride

Guidance literature:: With hydrogenchloride; 3 A molecular sieve; sodium cyanoborohydride; In methanol; for 48h; Heating;
DOI:10.1021/jm00384a017

Reference yield:

: 92532-21-3
1-(3-hydroxyphenyl)-1-hexanol

: 92532-27-9
benzyl 3-<1-(N-methylamino)hexyl>phenyl ether hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: NaI, Cs₂CO₃ / acetone / 18 h / Heating

2: 98 percent / pyridinium chlorochromate / CH₂Cl₂ / 1.5 h / Ambient temperature

3: 41 percent / sodium cyanoborohydride, HCl, molecular sieves 3A / methanol / 48 h / Heating

With hydrogenchloride; 3 A molecular sieve; sodium cyanoborohydride; caesium carbonate; pyridinium chlorochromate; sodium iodide; In methanol; dichloromethane; acetone;
DOI:10.1021/jm00384a017

Reference yield:

: 693-25-4
n-pentylmagnesium bromide

: 92532-27-9
benzyl 3-<1-(N-methylamino)hexyl>phenyl ether hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: diethyl ether / 0 - 20 °C

2: NaI, Cs₂CO₃ / acetone / 18 h / Heating

3: 98 percent / pyridinium chlorochromate / CH₂Cl₂ / 1.5 h / Ambient temperature

4: 41 percent / sodium cyanoborohydride, HCl, molecular sieves 3A / methanol / 48 h / Heating

With hydrogenchloride; 3 A molecular sieve; sodium cyanoborohydride; caesium carbonate; pyridinium chlorochromate; sodium iodide; In methanol; diethyl ether; dichloromethane; acetone;
DOI:10.1021/jm00384a017