2-((1R,5R)-5-((4-methoxybenzyl)oxy)cyclopent-2-en-1-yl)-N,N-dimethylacetamide

Base Information

Chemical Name:2-((1R,5R)-5-((4-methoxybenzyl)oxy)cyclopent-2-en-1-yl)-N,N-dimethylacetamide
CAS No.:1605291-78-8
Molecular Formula:C₁₇H₂₃NO₃
Molecular Weight:289.375
Hs Code.:

Synonyms:2-((1R,5R)-5-((4-methoxybenzyl)oxy)cyclopent-2-en-1-yl)-N,N-dimethylacetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-((1R,5R)-5-((4-methoxybenzyl)oxy)cyclopent-2-en-1-yl)-N,N-dimethylacetamide

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Technology Process of 2-((1R,5R)-5-((4-methoxybenzyl)oxy)cyclopent-2-en-1-yl)-N,N-dimethylacetamide

There total 1 articles about 2-((1R,5R)-5-((4-methoxybenzyl)oxy)cyclopent-2-en-1-yl)-N,N-dimethylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 18871-66-4
N,N-dimethylacetamide dimethyl acetal

: 1514903-06-0
(1R,4R)-4-((4-methoxybenzyl)oxy)cyclopent-2-enol

: 1605291-78-8
2-((1R,5R)-5-((4-methoxybenzyl)oxy)cyclopent-2-en-1-yl)-N,N-dimethylacetamide

Guidance literature:: In para-xylene; for 1h; Reflux;
DOI:10.1021/ol500654g

Reference yield: 80.0%

: 1605291-78-8
2-((1R,5R)-5-((4-methoxybenzyl)oxy)cyclopent-2-en-1-yl)-N,N-dimethylacetamide

: 1605291-79-9
2-((1R,5R)-5-((4-methoxybenzyl)oxy)cyclopent-2-en-1-yl)acetaldehyde

Guidance literature:: With diisobutylaluminium hydride; In tetrahydrofuran; hexane; at -105 ℃; for 1h; Temperature;
DOI:10.1021/ol500654g

Reference yield:

: 1605291-78-8
2-((1R,5R)-5-((4-methoxybenzyl)oxy)cyclopent-2-en-1-yl)-N,N-dimethylacetamide

: 123-11-5
4-methoxy-benzaldehyde

Guidance literature:: Multi-step reaction with 5 steps

1.1: diisobutylaluminium hydride / tetrahydrofuran; hexane / 1 h / -105 °C

2.1: triphenylphosphine / dichloromethane / 0.17 h / 0 °C

3.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C

4.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C

4.2: 2 h / -78 - 20 °C

5.1: triethylamine; N-Bromosuccinimide / dimethyl sulfoxide; water / 12 h / 0 - 20 °C

With N-Bromosuccinimide; n-butyllithium; diisobutylaluminium hydride; triethylamine; triphenylphosphine; In tetrahydrofuran; hexane; dichloromethane; water; dimethyl sulfoxide; 2.1: |Corey-Fuchs Alkyne Synthesis;
DOI:10.1021/ol500654g