meso-4,6-Di-O-benzyl-D-myo-inositol-1,3,5-tri(dimethyl phosphate)-2-(didecyl phosphate)

Base Information

Chemical Name:meso-4,6-Di-O-benzyl-D-myo-inositol-1,3,5-tri(dimethyl phosphate)-2-(didecyl phosphate)
CAS No.:1374660-13-5
Molecular Formula:C₄₆H₈₀O₁₈P₄
Molecular Weight:1045.03
Hs Code.:

Synonyms:meso-4,6-Di-O-benzyl-D-myo-inositol-1,3,5-tri(dimethyl phosphate)-2-(didecyl phosphate)

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Chemical Property of meso-4,6-Di-O-benzyl-D-myo-inositol-1,3,5-tri(dimethyl phosphate)-2-(didecyl phosphate)

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Technology Process of meso-4,6-Di-O-benzyl-D-myo-inositol-1,3,5-tri(dimethyl phosphate)-2-(didecyl phosphate)

There total 9 articles about meso-4,6-Di-O-benzyl-D-myo-inositol-1,3,5-tri(dimethyl phosphate)-2-(didecyl phosphate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1374659-99-0
meso-4,6-di-O-benzyl-D-myo-inositol-2-(didecyl phosphate)

: 122194-07-4
dimethyl N,N-diisopropylphosphoramidite

: 1374660-13-5
meso-4,6-Di-O-benzyl-D-myo-inositol-1,3,5-tri(dimethyl phosphate)-2-(didecyl phosphate)

Guidance literature:: dimethyl N,N-diisopropylphosphoramidite; With 1H-tetrazole; In dichloromethane; for 0.5h; Inert atmosphere;

meso-4,6-di-O-benzyl-D-myo-inositol-2-(didecyl phosphate); In dichloromethane; at 20 ℃; Inert atmosphere;

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; Cooling with ice; Inert atmosphere;

Reference yield:

: C₄₆H₈₀O₁₅P₄

: 1374660-13-5
meso-4,6-Di-O-benzyl-D-myo-inositol-1,3,5-tri(dimethyl phosphate)-2-(didecyl phosphate)

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 - 20 ℃; for 2h; Inert atmosphere;
DOI:10.1039/c2ob00031h

Reference yield:

: meso-4,6-di-O-benzyl-1,3,5-O-orthoformate-D-myo-inositol-2-(didecyl phosphate)

: 1374660-13-5
meso-4,6-Di-O-benzyl-D-myo-inositol-1,3,5-tri(dimethyl phosphate)-2-(didecyl phosphate)

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride / methanol / 7 h / 20 - 35 °C

2.1: 1H-tetrazole / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

2.2: Inert atmosphere

3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

With 1H-tetrazole; hydrogenchloride; 3-chloro-benzenecarboperoxoic acid; In methanol; dichloromethane;
DOI:10.1039/c2ob00031h