2-([(4-METHOXYPHENYL)SULFONYL]AMINO)-2-PHENYLACETIC ACID

Base Information

• Chemical Name: 2-([(4-METHOXYPHENYL)SULFONYL]AMINO)-2-PHENYLACETIC ACID
• CAS No.: 117309-46-3
• Molecular Formula: C15H15 N O5 S
• Molecular Weight: 321.35
• Hs Code.: 2935009090
• Mol file: 117309-46-3.mol

Synonyms:2-([(4-METHOXYPHENYL)SULFONYL]AMINO)-2-PHENYLACETIC ACID

Chemical Property of 2-([(4-METHOXYPHENYL)SULFONYL]AMINO)-2-PHENYLACETIC ACID

Chemical Property:

• Vapor Pressure: 8.34E-12mmHg at 25°C
• Melting Point: 171-173°C
• Boiling Point: 523.9°Cat760mmHg
• Flash Point: 270.7°C
• PSA: 101.08000
• Density: 1.358g/cm³
• LogP: 3.27110

Purity/Quality:

97% ^*data from raw suppliers

2-{[(4-Methoxyphenyl)sulfonyl]amino}-2-phenylacetic acid >95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-([(4-METHOXYPHENYL)SULFONYL]AMINO)-2-PHENYLACETIC ACID

There total 2 articles about 2-([(4-METHOXYPHENYL)SULFONYL]AMINO)-2-PHENYLACETIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 14.0%

(S)-2-phenylglycine (2935-35-5) + 4-methoxy-phenyl-sulphonyl chloride (98-68-0) → (S)-(4-Methoxy-benzenesulfonylamino)-phenyl-acetic acid (117309-46-3)

Guidance literature:

With sodium hydroxide; In tetrahydrofuran; water; at 70 - 80 ℃; for 0.5h;

DOI:10.1021/jm00121a027

Reference yield:

C17H17NO5S → (S)-(4-Methoxy-benzenesulfonylamino)-phenyl-acetic acid (117309-46-3)

Guidance literature:

With ruthenium trichloride; periodic acid; In water; acetonitrile; at 20 ℃; for 24h; Inert atmosphere;

DOI:10.1021/ja805122j

Reference yield:

methanol (67-56-1) + (S)-(4-Methoxy-benzenesulfonylamino)-phenyl-acetic acid (117309-46-3) → C16H17NO5S

Guidance literature:

With chloro-trimethyl-silane; at 20 ℃; for 12h; Inert atmosphere;

DOI:10.1021/ja805122j

upstream raw materials:

(S)-2-phenylglycine

4-methoxy-phenyl-sulphonyl chloride

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