2-(4-methylphenyl)-3-methylbenzothiophene

Base Information

Chemical Name:2-(4-methylphenyl)-3-methylbenzothiophene
CAS No.:1276113-97-3
Molecular Formula:C₁₆H₁₄S
Molecular Weight:238.353
Hs Code.:

Synonyms:2-(4-methylphenyl)-3-methylbenzothiophene

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Chemical Property of 2-(4-methylphenyl)-3-methylbenzothiophene

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Technology Process of 2-(4-methylphenyl)-3-methylbenzothiophene

There total 3 articles about 2-(4-methylphenyl)-3-methylbenzothiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1455-18-1
3-methylbenzothiophene

: 624-31-7
4-tolyl iodide

: 1276113-97-3
2-(4-methylphenyl)-3-methylbenzothiophene

Guidance literature:: With 1,1,1,3',3',3'-hexafluoro-propanol; sodium acetate; palladium diacetate; silver(l) oxide; at 30 ℃; for 16h;
DOI:10.1021/jacs.8b05361

Reference yield: 85.0%

: 1455-18-1
3-methylbenzothiophene

: 106-38-7
para-bromotoluene

: 1276113-97-3
2-(4-methylphenyl)-3-methylbenzothiophene

Guidance literature:: With (3-phenylallyl)(chloro)-[1,3-bis(2,6-diisopropylphenyl)-4,5-dihydroimidazol-2-ylidene]palladium(II); potassium carbonate; trimethylpyruvic acid; In N,N-dimethyl acetamide; at 140 ℃; for 16h;
DOI:10.3762/bjoc.8.187

Reference yield: 82.0%

: 3133-78-6
3-methylbenzo[b]thiophene-2-carboxylic acid

: 29540-83-8
p-tolyl triflate

: 1276113-97-3
2-(4-methylphenyl)-3-methylbenzothiophene

Guidance literature:: With (1,10-phenanthroline)bis(triphenylphosphine)copper(I) nitrate; potassium tert-butylate; palladium diacetate; In 1-methyl-pyrrolidin-2-one; at 170 ℃; for 1h; Sonication; Continuous flow reactor;
DOI:10.1039/c0cc05708h