1-<<3-(2-guanidino-4-thiazolyl)phenyl>amino>-1-(methylthio)-2-nitroethene

Base Information

Chemical Name:1-<<3-(2-guanidino-4-thiazolyl)phenyl>amino>-1-(methylthio)-2-nitroethene
CAS No.:83844-78-4
Molecular Formula:C₁₃H₁₄N₆O₂S₂
Molecular Weight:350.425
Hs Code.:

Synonyms:1-<<3-(2-guanidino-4-thiazolyl)phenyl>amino>-1-(methylthio)-2-nitroethene

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Chemical Property of 1-<<3-(2-guanidino-4-thiazolyl)phenyl>amino>-1-(methylthio)-2-nitroethene

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Technology Process of 1-<<3-(2-guanidino-4-thiazolyl)phenyl>amino>-1-(methylthio)-2-nitroethene

There total 4 articles about 1-<<3-(2-guanidino-4-thiazolyl)phenyl>amino>-1-(methylthio)-2-nitroethene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 72801-60-6
2-guanidino-4-(3-aminophenyl)thiazole

: 13623-94-4
1,1-di(methylsulfanyl)-2-nitroethylene

: 83844-78-4
1-<<3-(2-guanidino-4-thiazolyl)phenyl>amino>-1-(methylthio)-2-nitroethene

Guidance literature:: In acetonitrile; for 2h; Heating;
DOI:10.1021/jm00356a005

Reference yield:

: 83831-32-7
2-guanidino-4-(3-nitrophenyl)thiazole

: 83844-78-4
1-<<3-(2-guanidino-4-thiazolyl)phenyl>amino>-1-(methylthio)-2-nitroethene

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / H₂, concd. HCl / 10percent Pd/C / ethanol / 4 h / 2585.7 Torr

2: 82 percent / acetonitrile / 2 h / Heating

With hydrogenchloride; hydrogen; palladium on activated charcoal; In ethanol; acetonitrile;
DOI:10.1021/jm00356a005

Reference yield:

: 2227-64-7
3'-nitro-2-bromoacetophenone

: 83844-78-4
1-<<3-(2-guanidino-4-thiazolyl)phenyl>amino>-1-(methylthio)-2-nitroethene

Guidance literature:: Multi-step reaction with 3 steps

1: 59 percent / triethylamine / methanol / Ambient temperature

2: 85 percent / H₂, concd. HCl / 10percent Pd/C / ethanol / 4 h / 2585.7 Torr

3: 82 percent / acetonitrile / 2 h / Heating

With hydrogenchloride; hydrogen; triethylamine; palladium on activated charcoal; In methanol; ethanol; acetonitrile;
DOI:10.1021/jm00356a005