(+/-)-2-O-acetoxy-4-(tert-butyldiphenylsilyloxymethyl)-3-phenylselenyltetrahydrothiophen

Base Information

Chemical Name:(+/-)-2-O-acetoxy-4-(tert-butyldiphenylsilyloxymethyl)-3-phenylselenyltetrahydrothiophen
CAS No.:381211-62-7
Molecular Formula:C₂₉H₃₄O₃SSeSi
Molecular Weight:569.699
Hs Code.:

Synonyms:(+/-)-2-O-acetoxy-4-(tert-butyldiphenylsilyloxymethyl)-3-phenylselenyltetrahydrothiophen

Suppliers and Price of (+/-)-2-O-acetoxy-4-(tert-butyldiphenylsilyloxymethyl)-3-phenylselenyltetrahydrothiophen

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-2-O-acetoxy-4-(tert-butyldiphenylsilyloxymethyl)-3-phenylselenyltetrahydrothiophen

Chemical Property:

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Technology Process of (+/-)-2-O-acetoxy-4-(tert-butyldiphenylsilyloxymethyl)-3-phenylselenyltetrahydrothiophen

There total 13 articles about (+/-)-2-O-acetoxy-4-(tert-butyldiphenylsilyloxymethyl)-3-phenylselenyltetrahydrothiophen which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 80904-75-2
4-hydroxymethyl-5H-furan-2-one

: 381211-62-7
(+/-)-2-O-acetoxy-4-(tert-butyldiphenylsilyloxymethyl)-3-phenylselenyltetrahydrothiophen

Guidance literature:: Multi-step reaction with 12 steps

1: 99 percent / H₂ / Pd/C

2: aq. NaOH

3: aq. NaOH

4: dicyclohexylcarbodiimide

5: LiHMDS

6: -78 °C

7: DIBAL

With sodium hydroxide; hydrogen; diisobutylaluminium hydride; dicyclohexyl-carbodiimide; lithium hexamethyldisilazane; palladium on activated charcoal;
DOI:10.1081/NCN-100002344

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 381211-62-7
(+/-)-2-O-acetoxy-4-(tert-butyldiphenylsilyloxymethyl)-3-phenylselenyltetrahydrothiophen

Guidance literature:: Multi-step reaction with 12 steps

1: 99 percent / H₂ / Pd/C

2: aq. NaOH

3: aq. NaOH

4: dicyclohexylcarbodiimide

5: LiHMDS

6: -78 °C

7: DIBAL

With sodium hydroxide; hydrogen; diisobutylaluminium hydride; dicyclohexyl-carbodiimide; lithium hexamethyldisilazane; palladium on activated charcoal;
DOI:10.1081/NCN-100002344

Reference yield:

: 212776-53-9
4-(tert-Butyl-diphenyl-silanyloxymethyl)-5H-furan-2-one

: 381211-62-7
(+/-)-2-O-acetoxy-4-(tert-butyldiphenylsilyloxymethyl)-3-phenylselenyltetrahydrothiophen

Guidance literature:: Multi-step reaction with 11 steps

1: 99 percent / H₂ / Pd/C

2: aq. NaOH

3: aq. NaOH

4: dicyclohexylcarbodiimide

5: LiHMDS

6: -78 °C

7: DIBAL

With sodium hydroxide; hydrogen; diisobutylaluminium hydride; dicyclohexyl-carbodiimide; lithium hexamethyldisilazane; palladium on activated charcoal;
DOI:10.1081/NCN-100002344