3-[4-({3-[(E,Z)-{[2-(dimethylamino)ethoxy]imino}(phenyl)methyl]benzyl}oxy)phenyl]propanoic acid

Base Information

Chemical Name:3-[4-({3-[(E,Z)-{[2-(dimethylamino)ethoxy]imino}(phenyl)methyl]benzyl}oxy)phenyl]propanoic acid
CAS No.:1356598-67-8
Molecular Formula:C₂₇H₃₀N₂O₄
Molecular Weight:446.546
Hs Code.:

Synonyms:3-[4-({3-[(E,Z)-{[2-(dimethylamino)ethoxy]imino}(phenyl)methyl]benzyl}oxy)phenyl]propanoic acid

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Chemical Property of 3-[4-({3-[(E,Z)-{[2-(dimethylamino)ethoxy]imino}(phenyl)methyl]benzyl}oxy)phenyl]propanoic acid

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Technology Process of 3-[4-({3-[(E,Z)-{[2-(dimethylamino)ethoxy]imino}(phenyl)methyl]benzyl}oxy)phenyl]propanoic acid

There total 6 articles about 3-[4-({3-[(E,Z)-{[2-(dimethylamino)ethoxy]imino}(phenyl)methyl]benzyl}oxy)phenyl]propanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5597-50-2
3-(4-hydroxyphenyl)propionic acid methyl ester

: 1356598-67-8
3-[4-({3-[(E,Z)-{[2-(dimethylamino)ethoxy]imino}(phenyl)methyl]benzyl}oxy)phenyl]propanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h / 20 °C

1.2: 24 h / 20 °C

2.1: hydroxylamine hydrochloride; pyridine / methanol / 3 h / 85 °C

3.1: sodium hydride / N,N-dimethyl-formamide; benzene / 0.25 h / 0 °C / Inert atmosphere

3.2: 3 h / 0 - 45 °C / Inert atmosphere

4.1: sodium hydroxide; water / tetrahydrofuran; methanol / 15 h / 20 °C

4.2: pH 3

With pyridine; hydroxylamine hydrochloride; water; sodium hydride; potassium carbonate; sodium hydroxide; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; benzene;

Reference yield:

: 1356600-02-6
methyl 3-[4-({3-[(E,Z)-{[2-(dimethylamino)ethoxy]imino}(phenyl)methyl]benzyl}oxy)phenyl]propanoate

: 1356598-67-8
3-[4-({3-[(E,Z)-{[2-(dimethylamino)ethoxy]imino}(phenyl)methyl]benzyl}oxy)phenyl]propanoic acid

Guidance literature:: methyl 3-[4-({3-[(E,Z)-{[2-(dimethylamino)ethoxy]imino}(phenyl)methyl]benzyl}oxy)phenyl]propanoate; With water; sodium hydroxide; In tetrahydrofuran; methanol; at 20 ℃; for 15h;

With hydrogenchloride; In tetrahydrofuran; methanol; water; pH=3;

Reference yield:

: 501-97-3
4-hydroxyphenylpropionic acid

: 1356598-67-8
3-[4-({3-[(E,Z)-{[2-(dimethylamino)ethoxy]imino}(phenyl)methyl]benzyl}oxy)phenyl]propanoic acid

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h / 20 °C

1.2: 3 h / 0 - 20 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h / 20 °C

2.2: 24 h / 20 °C

3.1: hydroxylamine hydrochloride; pyridine / methanol / 3 h / 85 °C

4.1: sodium hydride / N,N-dimethyl-formamide; benzene / 0.25 h / 0 °C / Inert atmosphere

4.2: 3 h / 0 - 45 °C / Inert atmosphere

5.1: sodium hydroxide; water / tetrahydrofuran; methanol / 15 h / 20 °C

5.2: pH 3

With pyridine; hydroxylamine hydrochloride; water; sodium hydride; potassium carbonate; sodium hydroxide; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; benzene;