tert-butyl N2-[(9H-fluoren-9-ylmethoxy)carbonyl]-N1-[2-(4-fluorophenyl)-1,1-dimethylethyl]-L-α-glutaminate

Base Information

• Chemical Name: tert-butyl N2-[(9H-fluoren-9-ylmethoxy)carbonyl]-N1-[2-(4-fluorophenyl)-1,1-dimethylethyl]-L-α-glutaminate
• CAS No.: 920289-26-5
• Molecular Formula: C₃₄H₃₉FN₂O₅
• Molecular Weight: 574.692

Synonyms:tert-butyl N2-[(9H-fluoren-9-ylmethoxy)carbonyl]-N1-[2-(4-fluorophenyl)-1,1-dimethylethyl]-L-α-glutaminate

Chemical Property of tert-butyl N2-[(9H-fluoren-9-ylmethoxy)carbonyl]-N1-[2-(4-fluorophenyl)-1,1-dimethylethyl]-L-α-glutaminate

Chemical Property:

Purity/Quality:

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• Pictogram(s):  
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Useful:

Technology Process of tert-butyl N2-[(9H-fluoren-9-ylmethoxy)carbonyl]-N1-[2-(4-fluorophenyl)-1,1-dimethylethyl]-L-α-glutaminate

There total 3 articles about tert-butyl N2-[(9H-fluoren-9-ylmethoxy)carbonyl]-N1-[2-(4-fluorophenyl)-1,1-dimethylethyl]-L-α-glutaminate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(4-fluoro-phenyl)-1,1-dimethyl-ethylamine hydrochloride (2413-54-9) + C29H35NO8 → tert-butyl N2-[(9H-fluoren-9-ylmethoxy)carbonyl]-N1-[2-(4-fluorophenyl)-1,1-dimethylethyl]-L-α-glutaminate (920289-26-5)

Guidance literature:

In toluene; at 5 - 15 ℃; for 1h; Product distribution / selectivity;

Reference yield:

C24H26ClNO5 + 1-(4-fluorophenyl)-2-methylpropan-2-amine (1200-27-7) → tert-butyl N2-[(9H-fluoren-9-ylmethoxy)carbonyl]-N1-[2-(4-fluorophenyl)-1,1-dimethylethyl]-L-α-glutaminate (920289-26-5)

Guidance literature:

In tetrahydrofuran; Product distribution / selectivity;

Reference yield:

→ tert-butyl N2-[(9H-fluoren-9-ylmethoxy)carbonyl]-N1-[2-(4-fluorophenyl)-1,1-dimethylethyl]-L-α-glutaminate (920289-26-5)

Guidance literature:

upstream raw materials:

2-(4-fluoro-phenyl)-1,1-dimethyl-ethylamine hydrochloride

1-(4-fluorophenyl)-2-methylpropan-2-amine

Downstream raw materials:

4(S)-Amino-4-[2-(4-fluoro-phenyl)-1,1-dimethyl-ethylcarbamoyl]-butyric acid tert-butyl ester

N-(1,1'-biphenyl-4-ylcarbonyl)-L-glutamic acid

1-(4-fluorophenyl)-2-methylpropan-2-amine

4(S)-[(Biphenyl-4-carbonyl)-amino]-4-[2-(4-fluoro-phenyl)-1,1-dimethyl-ethylcarbamoyl]-butyric acid

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