C₇₂H₉₄F₂O₁₂Si₃

Base Information

Chemical Name:C₇₂H₉₄F₂O₁₂Si₃
CAS No.:1332755-78-8
Molecular Formula:C₇₂H₉₄F₂O₁₂Si₃
Molecular Weight:1273.78
Hs Code.:

C<sub>72</sub>H<sub>94</sub>F<sub>2</sub>O<sub>12</sub>Si<sub>3</sub>

Synonyms:C₇₂H₉₄F₂O₁₂Si₃

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Chemical Property of C₇₂H₉₄F₂O₁₂Si₃

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Technology Process of C₇₂H₉₄F₂O₁₂Si₃

There total 19 articles about C₇₂H₉₄F₂O₁₂Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1873-88-7
1,1,1,3,5,5,5-heptamethyltrisiloxan

: 1332755-94-8
C₆₅H₇₂F₂O₁₀

: 1332755-78-8
C₇₂H₉₄F₂O₁₂Si₃

Guidance literature:: With platinum⁽⁰⁾-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex; In 5,5-dimethyl-1,3-cyclohexadiene; toluene; at 70 ℃;
DOI:10.1021/ja205550b

Reference yield:

: 94-18-8
Benzyl 4-hydroxybenzoate

: 1332755-78-8
C₇₂H₉₄F₂O₁₂Si₃

Guidance literature:: Multi-step reaction with 5 steps

1: di-isopropyl azodicarboxylate; triethylamine; triphenylphosphine / tetrahydrofuran / 20 °C / Inert atmosphere; Cooling with ice

2: dmap; dicyclohexyl-carbodiimide / dichloromethane / 16 h / 20 °C / Inert atmosphere

3: sodium chlorite; sodium dihydrogen phosphate monohydrate; recorcinol / tetrahydrofuran; water; tert-butyl alcohol / 20 °C

4: dmap; dicyclohexyl-carbodiimide / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere

5: platinum⁽⁰⁾-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex / 5,5-dimethyl-1,3-cyclohexadiene; toluene / 70 °C

With dmap; sodium chlorite; sodium dihydrogen phosphate monohydrate; platinum⁽⁰⁾-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex; di-isopropyl azodicarboxylate; triethylamine; dicyclohexyl-carbodiimide; triphenylphosphine; recorcinol; In tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene; dichloromethane; water; toluene; tert-butyl alcohol;
DOI:10.1021/ja205550b

Reference yield:

: 1332755-86-8
4-(benzyloxycarbonyl)phenyl 4-tetradecyloxy-2,3-difluorobenzoate

: 1332755-78-8
C₇₂H₉₄F₂O₁₂Si₃

Guidance literature:: Multi-step reaction with 5 steps

1: palladium 10% on activated carbon; hydrogen / tetrahydrofuran

2: dmap; dicyclohexyl-carbodiimide / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere

3: palladium 10% on activated carbon; hydrogen / tetrahydrofuran

4: dmap; dicyclohexyl-carbodiimide / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere

5: platinum⁽⁰⁾-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex / 5,5-dimethyl-1,3-cyclohexadiene; toluene / 70 °C

With dmap; platinum⁽⁰⁾-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex; palladium 10% on activated carbon; hydrogen; dicyclohexyl-carbodiimide; In tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene; toluene;
DOI:10.1021/ja205550b