Technology Process of C23H21N3O
There total 10 articles about C23H21N3O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
trifluoroacetic acid; ascorbic acid;
In
water;
at 20 ℃;
for 0.25h;
Inert atmosphere;
DOI:10.1039/c3ob42379d
- Guidance literature:
-
Multi-step reaction with 10 steps
1: 24 h / Inert atmosphere; Reflux
2: ammonium formate; 20% palladium hydroxide-activated charcoal / methanol; ethyl acetate / 3 h / Inert atmosphere; Reflux
3: triethylamine / dichloromethane / 23 °C / Inert atmosphere
4: trichlorophosphate / 6 h / Inert atmosphere; Reflux
5: hydrogen bromide / 72 h / Inert atmosphere; Reflux
6: tert-butyl alcohol / 48 h / 23 °C / Inert atmosphere
7: potassium carbonate / toluene; acetone / 8 h / Inert atmosphere; Reflux
8: tetrahydrofuran / 120 h / Inert atmosphere; Reflux
9: sodium cyanoborohydride / methanol / 3 h / 23 °C / Inert atmosphere
10: trifluoroacetic acid; ascorbic acid / water / 0.25 h / 20 °C / Inert atmosphere
With
20% palladium hydroxide-activated charcoal; hydrogen bromide; ammonium formate; sodium cyanoborohydride; potassium carbonate; triethylamine; trifluoroacetic acid; ascorbic acid; trichlorophosphate;
In
tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; acetone; toluene; tert-butyl alcohol;
DOI:10.1039/c3ob42379d
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium carbonate / toluene; acetone / 8 h / Inert atmosphere; Reflux
2: tetrahydrofuran / 120 h / Inert atmosphere; Reflux
3: sodium cyanoborohydride / methanol / 3 h / 23 °C / Inert atmosphere
4: trifluoroacetic acid; ascorbic acid / water / 0.25 h / 20 °C / Inert atmosphere
With
sodium cyanoborohydride; potassium carbonate; trifluoroacetic acid; ascorbic acid;
In
tetrahydrofuran; methanol; water; acetone; toluene;
DOI:10.1039/c3ob42379d
