di-tert-butyl 6-(4-(prop-2-ynyloxy)phenyl)phenanthridine-3,8-diyldicarbamate

Base Information

Chemical Name:di-tert-butyl 6-(4-(prop-2-ynyloxy)phenyl)phenanthridine-3,8-diyldicarbamate
CAS No.:1314081-05-4
Molecular Formula:C₃₂H₃₃N₃O₅
Molecular Weight:539.631
Hs Code.:

Synonyms:di-tert-butyl 6-(4-(prop-2-ynyloxy)phenyl)phenanthridine-3,8-diyldicarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of di-tert-butyl 6-(4-(prop-2-ynyloxy)phenyl)phenanthridine-3,8-diyldicarbamate

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Technology Process of di-tert-butyl 6-(4-(prop-2-ynyloxy)phenyl)phenanthridine-3,8-diyldicarbamate

There total 8 articles about di-tert-butyl 6-(4-(prop-2-ynyloxy)phenyl)phenanthridine-3,8-diyldicarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1314081-04-3
di-tert-butyl [6-(4-hydroxyphenyl)phenanthridine-3,8-diyl]dicarbamate

: 106-96-7
propargyl bromide

: 1314081-05-4
di-tert-butyl 6-(4-(prop-2-ynyloxy)phenyl)phenanthridine-3,8-diyldicarbamate

Guidance literature:: With potassium carbonate; In acetone; toluene; for 8h; Inert atmosphere; Reflux;
DOI:10.1039/c3ob42379d

Reference yield:

: 100-07-2
4-methoxy-benzoyl chloride

: 1314081-05-4
di-tert-butyl 6-(4-(prop-2-ynyloxy)phenyl)phenanthridine-3,8-diyldicarbamate

Guidance literature:: Multi-step reaction with 7 steps

1: chlorobenzene / Reflux

2: ammonium formate / 20 % Pd(OH)2/C

4: trichlorophosphate

5: hydrogen bromide / water

7: potassium carbonate / acetone

With hydrogen bromide; ammonium formate; potassium carbonate; trichlorophosphate; 20 % Pd(OH)2/C; In water; chlorobenzene; acetone;

Reference yield:

: 51787-75-8
4,4'-dinitro-2-biphenylamine

: 1314081-05-4
di-tert-butyl 6-(4-(prop-2-ynyloxy)phenyl)phenanthridine-3,8-diyldicarbamate

Guidance literature:: Multi-step reaction with 7 steps

1: chlorobenzene / Reflux

2: ammonium formate / 20 % Pd(OH)2/C

4: trichlorophosphate

5: hydrogen bromide / water

7: potassium carbonate / acetone

With hydrogen bromide; ammonium formate; potassium carbonate; trichlorophosphate; 20 % Pd(OH)2/C; In water; chlorobenzene; acetone;