Technology Process of (1E,2E)-3-(2,3-dichlorophenyl)-2-(2-methyl-1,3-dioxolan-2-yl)acrylaldehyde O-allyl oxime
There total 6 articles about (1E,2E)-3-(2,3-dichlorophenyl)-2-(2-methyl-1,3-dioxolan-2-yl)acrylaldehyde O-allyl oxime which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
acetone;
Reflux;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: toluene-4-sulfonic acid / toluene / 6 h / Reflux
2.1: diisobutylaluminium hydride / dichloromethane; hexanes / -78 - 20 °C
2.2: 0.25 h / 20 °C
3.1: pyridinium chlorochromate / dichloromethane / 2 h / 20 °C
4.1: hydroxylamine hydrochloride; pyridine / methanol / 20 °C
5.1: potassium carbonate / acetone / Reflux
With
pyridine; hydroxylamine hydrochloride; diisobutylaluminium hydride; potassium carbonate; toluene-4-sulfonic acid; pyridinium chlorochromate;
In
methanol; hexanes; dichloromethane; acetone; toluene;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: piperidine; 2-Picolinic acid / isopropyl alcohol / 45 °C
2.1: toluene-4-sulfonic acid / toluene / 6 h / Reflux
3.1: diisobutylaluminium hydride / dichloromethane; hexanes / -78 - 20 °C
3.2: 0.25 h / 20 °C
4.1: pyridinium chlorochromate / dichloromethane / 2 h / 20 °C
5.1: hydroxylamine hydrochloride; pyridine / methanol / 20 °C
6.1: potassium carbonate / acetone / Reflux
With
piperidine; pyridine; 2-Picolinic acid; hydroxylamine hydrochloride; diisobutylaluminium hydride; potassium carbonate; toluene-4-sulfonic acid; pyridinium chlorochromate;
In
methanol; hexanes; dichloromethane; isopropyl alcohol; acetone; toluene;
