(2-bromoethoxy)cyclohexane

Base Information

• Chemical Name: (2-bromoethoxy)cyclohexane
• CAS No.: 131665-94-6
• Molecular Formula: C₈H₁₅BrO
• Molecular Weight: 207.111
• Mol file: 131665-94-6.mol

Synonyms:(2-bromoethoxy)cyclohexane

Chemical Property of (2-bromoethoxy)cyclohexane

Chemical Property:

• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

(2-Bromoethoxy)cyclohexane ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (2-bromoethoxy)cyclohexane

There total 4 articles about (2-bromoethoxy)cyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

2-[2-(cyclohexoxy)ethyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane → (2-bromoethoxy)cyclohexane (131665-94-6)

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; 2-methoxybenzo[d][1,3,2]dioxaborole; benzenesulfonyl bromide; In methanol; dichloromethane; benzene; at 70 ℃; for 16h; Inert atmosphere;

DOI:10.1002/anie.202004012

Reference yield: 26.0%

2-Cyclohexyloxyethanol (1817-88-5) → (2-bromoethoxy)cyclohexane (131665-94-6)

Guidance literature:

With carbon tetrabromide; triphenylphosphine; In dichloromethane; at 20 ℃; Cooling with ice;

Reference yield: 10.0%

2-bromoethanol (540-51-2) + cyclohexene (110-83-8) → (2-bromoethoxy)cyclohexane (131665-94-6)

Guidance literature:

With (triphenylphosphine)silver(I) triflate; silver trifluoromethanesulfonate; triphenylphosphine; In toluene; at 85 ℃; for 24h; Inert atmosphere; Sealed tube;

upstream raw materials:

2-bromoethanol

cyclohexene

2-Cyclohexyloxyethanol

vinyl cyclohexyl ether

Downstream raw materials:

cyclohexene