SCH 71450

Base Information

Chemical Name:SCH 71450
CAS No.:1440545-91-4
Molecular Formula:C₂₂H₂₇NO₈
Molecular Weight:433.458
Hs Code.:

Synonyms:SCH 71450

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of SCH 71450

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Technology Process of SCH 71450

There total 12 articles about SCH 71450 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: C₄₄H₄₅NO₁₀

: 1440545-91-4
SCH 71450

Guidance literature:: With hydrogen; palladium(II) hydroxide; In tetrahydrofuran; methanol; at 20 ℃; for 4.5h;
DOI:10.1002/ejoc.201300072

Reference yield:

: C₅₂H₅₃NO₁₄

: 1440545-91-4
SCH 71450

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / methanol; tetrahydrofuran / 1 h / 20 °C

2: palladium(II) hydroxide; hydrogen / methanol; tetrahydrofuran / 4.5 h / 20 °C

With hydrogen; palladium(II) hydroxide; potassium carbonate; In tetrahydrofuran; methanol;
DOI:10.1002/ejoc.201300072

Reference yield:

: 851318-54-2
allyl (p-allyloxyphenyl)acetate

: 1440545-91-4
SCH 71450

Guidance literature:: Multi-step reaction with 10 steps

1.1: sodium hydroxide / methanol / 2 h / 35 °C

2.1: oxalyl dichloride / 2 h / 20 °C

3.1: sodium hydroxide / dichloromethane / 20 °C

4.1: trichlorophosphate / acetonitrile / 1 h / 90 °C

5.1: chloro {[(1S,2S)-(+)-2-amino-1,2-diphenylethyl]((4-toluenesulfonyl)amido)(p-cymene)}ruthenium(ll); / N,N-dimethyl-formamide / 2 h / 0 - 20 °C

6.1: triethylamine; dmap / dichloromethane / 1.5 h / 10 - 50 °C

7.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / methanol; tetrahydrofuran / 0.17 h / Inert atmosphere

7.2: 3 h / 68 °C / Inert atmosphere

8.1: dichloromethane / 1 h / -10 °C / Molecular sieve

8.2: 2.5 h / -10 °C

9.1: potassium carbonate / methanol; tetrahydrofuran / 1 h / 20 °C

10.1: palladium(II) hydroxide; hydrogen / methanol; tetrahydrofuran / 4.5 h / 20 °C

With dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; oxalyl dichloride; chloro {[(1S,2S)-(+)-2-amino-1,2-diphenylethyl]((4-toluenesulfonyl)amido)(p-cymene)}ruthenium(ll); hydrogen; palladium(II) hydroxide; potassium carbonate; triethylamine; sodium hydroxide; trichlorophosphate; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile; 4.1: |Bischler-Napieralski Reaction;
DOI:10.1002/ejoc.201300072