5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthyl-N-methoxy-N-methylamide

Base Information

Chemical Name:5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthyl-N-methoxy-N-methylamide
CAS No.:1178511-52-8
Molecular Formula:C₁₇H₂₅NO₂
Molecular Weight:275.391
Hs Code.:

Synonyms:5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthyl-N-methoxy-N-methylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthyl-N-methoxy-N-methylamide

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Technology Process of 5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthyl-N-methoxy-N-methylamide

There total 1 articles about 5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthyl-N-methoxy-N-methylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 104224-50-2
5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphtholyl chloride

: 1178511-52-8
5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthyl-N-methoxy-N-methylamide

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 17h;

Reference yield: 25.0%

: 108-86-1,52753-63-6
bromobenzene

: 1178511-52-8
5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthyl-N-methoxy-N-methylamide

: 102447-36-9
5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthyl phenyl ketone

Guidance literature:: bromobenzene; With magnesium; In tetrahydrofuran;

5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthyl-N-methoxy-N-methylamide; In tetrahydrofuran; diethyl ether; at 20 ℃; for 22h;

With water; ammonium chloride; In tetrahydrofuran; diethyl ether;
DOI:10.1016/j.bmc.2009.04.044