C₂₃H₃₈FNO₆SSi

Base Information

Chemical Name:C₂₃H₃₈FNO₆SSi
CAS No.:1198224-01-9
Molecular Formula:C₂₃H₃₈FNO₆SSi
Molecular Weight:503.708
Hs Code.:

C<sub>23</sub>H<sub>38</sub>FNO<sub>6</sub>SSi

Synonyms:C₂₃H₃₈FNO₆SSi

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Chemical Property of C₂₃H₃₈FNO₆SSi

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Technology Process of C₂₃H₃₈FNO₆SSi

There total 13 articles about C₂₃H₃₈FNO₆SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₁H₃₅ClFNO₄SSi

: 127-09-3
sodium acetate

: 1198224-01-9
C₂₃H₃₈FNO₆SSi

Guidance literature:: With sodium iodide; In N,N-dimethyl-formamide; at 80 ℃; for 8h;

Reference yield:

: 1198223-28-7
ethyl 3-cyclopentyloxy-4-fluorobenzoate

: 1198224-01-9
C₂₃H₃₈FNO₆SSi

Guidance literature:: Multi-step reaction with 11 steps

1.1: water; sodium hydroxide / ethanol / 3 h / 55 °C

2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 0.08 h / 20 °C

2.2: 13 h / 20 °C

3.1: tetrahydrofuran / 2.5 h / 0 °C

4.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / 0 °C

4.2: 3 h / -78 - 20 °C

5.1: potassium osmate(VI); water; potassium carbonate; hydroquinidein 1,4-phthalazinediyl diether; potassium hexacyanoferrate(III) / tert-butyl alcohol / 5 h / 0 °C

6.1: triethylamine / dichloromethane / 0.5 h / 0 - 20 °C

7.1: sodium azide / N,N-dimethyl-formamide / 15 h / 75 °C

8.1: 2,6-dimethylpyridine / 1 h / 20 °C

9.1: hydrogen / palladium 10% on activated carbon / methanol / 1 h / 20 °C

10.1: triethylamine / dichloromethane / 1.5 h / 0 - 20 °C

11.1: sodium iodide / N,N-dimethyl-formamide / 8 h / 80 °C

With 2,6-dimethylpyridine; potassium osmate(VI); sodium azide; water; hydrogen; sodium hexamethyldisilazane; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; hydroquinidein 1,4-phthalazinediyl diether; triethylamine; sodium iodide; sodium hydroxide; potassium hexacyanoferrate(III); palladium 10% on activated carbon; In tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; tert-butyl alcohol;

Reference yield:

: 1198282-76-6
C₁₄H₁₈FNO₃

: 1198224-01-9
C₂₃H₃₈FNO₆SSi

Guidance literature:: Multi-step reaction with 9 steps

1.1: tetrahydrofuran / 2.5 h / 0 °C

2.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / 0 °C

2.2: 3 h / -78 - 20 °C

3.1: potassium osmate(VI); water; potassium carbonate; hydroquinidein 1,4-phthalazinediyl diether; potassium hexacyanoferrate(III) / tert-butyl alcohol / 5 h / 0 °C

4.1: triethylamine / dichloromethane / 0.5 h / 0 - 20 °C

5.1: sodium azide / N,N-dimethyl-formamide / 15 h / 75 °C

6.1: 2,6-dimethylpyridine / 1 h / 20 °C

7.1: hydrogen / palladium 10% on activated carbon / methanol / 1 h / 20 °C

8.1: triethylamine / dichloromethane / 1.5 h / 0 - 20 °C

9.1: sodium iodide / N,N-dimethyl-formamide / 8 h / 80 °C

With 2,6-dimethylpyridine; potassium osmate(VI); sodium azide; water; hydrogen; sodium hexamethyldisilazane; potassium carbonate; hydroquinidein 1,4-phthalazinediyl diether; triethylamine; sodium iodide; potassium hexacyanoferrate(III); palladium 10% on activated carbon; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; tert-butyl alcohol;