NOJIRIMYCIN-1-SULFONIC ACID

Base Information

• Chemical Name: NOJIRIMYCIN-1-SULFONIC ACID
• CAS No.: 114417-84-4
• Molecular Formula: C₆H₁₃NO₇S
• Molecular Weight: 243.238
• Mol file: 114417-84-4.mol

Synonyms:2-Piperidinesulfonicacid, 3,4,5-trihydroxy-6-(hydroxymethyl)-, (3R,4S,5R,6R)-[partial]-;Nojirimycin bisulfite adduct; Nojirimycin sulfite adduct

Chemical Property of NOJIRIMYCIN-1-SULFONIC ACID

Chemical Property:

• Melting Point: 124-130掳C dec.
• Boiling Point: °Cat760mmHg
• PKA: -1.21±0.70(Predicted)
• Flash Point: °C
• PSA: 186.76000
• Density: 1.89g/cm³
• LogP: -2.41580
• Storage Temp.: -20°C Freezer
• Solubility.: Water (Sparingly, Heated)

Purity/Quality:

99% ^*data from raw suppliers

Nojirimycin-1-Sulfonic Acid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: An inhibitor of several glucosidases. Can be converted to Nojirimycin by treatment with Basic Resin.

Technology Process of NOJIRIMYCIN-1-SULFONIC ACID

There total 12 articles about NOJIRIMYCIN-1-SULFONIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

5-amino-5-deoxy-1,2-O-isoproylidene-6-O-trityl-α-D-galactofuranose (109681-00-7) → 5-amino-5-deoxy-D-galactopyranose hydrogensulfite adduct (78698-43-8,81703-56-2,91384-36-0,91384-37-1,109784-32-9,109784-33-0,109784-34-1,109784-35-2,114417-84-4,126575-58-4,130979-29-2,149406-06-4,149406-07-5)

Guidance literature:

With sulfur dioxide; In methanol; at 40 ℃; for 40h; sealed vessel;

DOI:10.1016/S0008-6215(00)90138-1

Reference yield: 68.0%

5-amino-5-deoxy-1,2-O-isoproylidene-6-O-trityl-β-L-altrofuranose (109681-01-8) → 5-amino-5-deoxy-L-altropyranose hydrogensulfite adduct (78698-43-8,81703-56-2,91384-36-0,91384-37-1,109784-32-9,109784-33-0,109784-34-1,109784-35-2,114417-84-4,126575-58-4,130979-29-2,149406-06-4,149406-07-5)

Guidance literature:

With sulfur dioxide; In methanol; at 40 ℃; for 40h;

DOI:10.1016/S0008-6215(00)90138-1

Reference yield: 67.0%

5-<(tert-Butoxycarbonyl)amino>-4-O-(tert-butyldimethylsilyl)-5-deoxy-2-O,3-O-isopropylidene-5-N,6-O-isopropylidene-D-galactose (168326-10-1) → 5-amino-5-deoxy-D-galactopyranose hydrogensulfite adduct (78698-43-8,81703-56-2,91384-36-0,91384-37-1,109784-32-9,109784-33-0,109784-34-1,109784-35-2,114417-84-4,126575-58-4,130979-29-2,149406-06-4,149406-07-5)

Guidance literature:

With sulfur dioxide; water; 1.) 40 deg C, 2 d, 2.) MeOH, 0 deg C, 12 h;

DOI:10.1021/jo00120a017

upstream raw materials:

(2R,3S,4S,5R)-2,3:4,6-bis(isopropylidenedioxy)-5-<<<(p-methoxybenzyl)oxy>carbonyl>amino>hexanal

5-amino-5-deoxy-1,2-O-isoproylidene-6-O-trityl-α-D-galactofuranose

5-<(tert-Butoxycarbonyl)amino>-4-O-(tert-butyldimethylsilyl)-5-deoxy-2-O,3-O-isopropylidene-5-N,6-O-isopropylidene-D-galactose

(2S,3S,4S,5R)-5-amino-2,3:4,6-bis(isopropylidenedioxy)hexan-1-ol

Downstream raw materials:

nojirimycin

5-amino-5-deoxy-L-altropyranose

(+)-Galactostatin

(+)-galactostatin

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