4-(1-tert-butoxycarbonyl-1-methylethoxy)-5-chloro-2-hydroxybenzoic acid methyl ester

Base Information

Chemical Name:4-(1-tert-butoxycarbonyl-1-methylethoxy)-5-chloro-2-hydroxybenzoic acid methyl ester
CAS No.:1003567-14-3
Molecular Formula:C₁₆H₂₁ClO₆
Molecular Weight:344.792
Hs Code.:

Synonyms:4-(1-tert-butoxycarbonyl-1-methylethoxy)-5-chloro-2-hydroxybenzoic acid methyl ester

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Chemical Property of 4-(1-tert-butoxycarbonyl-1-methylethoxy)-5-chloro-2-hydroxybenzoic acid methyl ester

Chemical Property:

Purity/Quality:

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MSDS Files:: SDS file from LookChem

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Technology Process of 4-(1-tert-butoxycarbonyl-1-methylethoxy)-5-chloro-2-hydroxybenzoic acid methyl ester

There total 2 articles about 4-(1-tert-butoxycarbonyl-1-methylethoxy)-5-chloro-2-hydroxybenzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.2%

: 23877-12-5
tert-butyl bromoisobutyrate

: 67828-69-7
methyl 5-chloro-2,4-dihydroxybenzoate

: 1003567-14-3
4-(1-tert-butoxycarbonyl-1-methylethoxy)-5-chloro-2-hydroxybenzoic acid methyl ester

: 585-07-9,25189-00-8
tert-Butyl methacrylate

Guidance literature:: tert-butyl bromoisobutyrate; methyl 5-chloro-2,4-dihydroxybenzoate; With tetrabutylammomium bromide; potassium carbonate; In 1-methyl-pyrrolidin-2-one; at 60 - 65 ℃; for 16h;

With hydrogenchloride; In 1-methyl-pyrrolidin-2-one; water; pH=~ 4;

Reference yield:

: 23877-12-5
tert-butyl bromoisobutyrate

: 67828-69-7
methyl 5-chloro-2,4-dihydroxybenzoate

: 1003567-14-3
4-(1-tert-butoxycarbonyl-1-methylethoxy)-5-chloro-2-hydroxybenzoic acid methyl ester

Guidance literature:: methyl 5-chloro-2,4-dihydroxybenzoate; With 2,6-di-tert-butyl-4-methyl-phenol; tetrabutylammomium bromide; potassium carbonate; In 1-methyl-pyrrolidin-2-one; for 0.5h; Inert atmosphere;

tert-butyl bromoisobutyrate; In 1-methyl-pyrrolidin-2-one; at 55 - 60 ℃; for 16h; Inert atmosphere;