(2S,3R,4S)-2<(tert-butyloxycarbonyl)amino>-1-cyclohexyl-3,4-dihydroxyhexane

Base Information

• Chemical Name: (2S,3R,4S)-2<(tert-butyloxycarbonyl)amino>-1-cyclohexyl-3,4-dihydroxyhexane
• CAS No.: 117248-32-5
• Molecular Formula: C₁₇H₃₃NO₄
• Molecular Weight: 315.453

Synonyms:(2S,3R,4S)-2<(tert-butyloxycarbonyl)amino>-1-cyclohexyl-3,4-dihydroxyhexane

Chemical Property of (2S,3R,4S)-2<(tert-butyloxycarbonyl)amino>-1-cyclohexyl-3,4-dihydroxyhexane

Chemical Property:

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Technology Process of (2S,3R,4S)-2<(tert-butyloxycarbonyl)amino>-1-cyclohexyl-3,4-dihydroxyhexane

There total 1 articles about (2S,3R,4S)-2<(tert-butyloxycarbonyl)amino>-1-cyclohexyl-3,4-dihydroxyhexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

((Z)-(S)-1-Cyclohexylmethyl-pent-2-enyl)-carbamic acid tert-butyl ester → (2S,3R,4S)-2-[(tert-butyloxycarbonyl)amino]-1-cyclohexyl-3,4-dihydroxy-6-methylheptane (104882-10-2) + (2S,3R,4S)-2<(tert-butyloxycarbonyl)amino>-1-cyclohexyl-3,4-dihydroxyhexane (117248-32-5) + (2S,3S,4S)-2<(tert-butyloxycarbonyl)amino>-1-cyclohexyl-3,4-dihydroxy-6-methylheptane (104974-39-2) + (2S,3R,4R)-2<(tert-butyloxycarbonyl)amino>-1-cyclohexyl-3,4-dihydroxy-6-methylheptane (104974-40-5)

Guidance literature:

With osmium(VIII) oxide; 4-methylmorpholine N-oxide; In tetrahydrofuran; tert-butyl alcohol; for 96h; Yields of byproduct given;

DOI:10.1021/jm00120a005

Reference yield:

(S)-N-(Ethoxycarbonyl)leucine (19887-30-0) + (2S,3R,4S)-2<(tert-butyloxycarbonyl)amino>-1-cyclohexyl-3,4-dihydroxyhexane (117248-32-5) + N-(tert-butoxycarbonyl)-L-histidine (17791-52-5) → {(S)-1-[(S)-1-((1S,2R,3S)-1-Cyclohexylmethyl-2,3-dihydroxy-pentylcarbamoyl)-2-(1H-imidazol-4-yl)-ethylcarbamoyl]-3-methyl-butyl}-carbamic acid ethyl ester

Guidance literature:

Yield given. Multistep reaction;

DOI:10.1021/jm00120a005

Reference yield:

(ethoxycarbonyl)-L-phenylalanine (19887-32-2) + (2S,3R,4S)-2<(tert-butyloxycarbonyl)amino>-1-cyclohexyl-3,4-dihydroxyhexane (117248-32-5) + N-(tert-butoxycarbonyl)-L-histidine (17791-52-5) → {(S)-1-[(S)-1-((1S,2R,3S)-1-Cyclohexylmethyl-2,3-dihydroxy-pentylcarbamoyl)-2-(1H-imidazol-4-yl)-ethylcarbamoyl]-2-phenyl-ethyl}-carbamic acid ethyl ester

Guidance literature:

Yield given. Multistep reaction;

DOI:10.1021/jm00120a005

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