(4S,5S)-3-Benzyloxycarbonyl-5-(2-chloroethyl)-4-isobutyl-2,2-dimethyloxazolidine

Base Information

Chemical Name:(4S,5S)-3-Benzyloxycarbonyl-5-(2-chloroethyl)-4-isobutyl-2,2-dimethyloxazolidine
CAS No.:116993-92-1
Molecular Formula:C₁₉H₂₈ClNO₃
Molecular Weight:353.889
Hs Code.:

Synonyms:(4S,5S)-3-Benzyloxycarbonyl-5-(2-chloroethyl)-4-isobutyl-2,2-dimethyloxazolidine

Suppliers and Price of (4S,5S)-3-Benzyloxycarbonyl-5-(2-chloroethyl)-4-isobutyl-2,2-dimethyloxazolidine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (4S,5S)-3-Benzyloxycarbonyl-5-(2-chloroethyl)-4-isobutyl-2,2-dimethyloxazolidine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (4S,5S)-3-Benzyloxycarbonyl-5-(2-chloroethyl)-4-isobutyl-2,2-dimethyloxazolidine

There total 6 articles about (4S,5S)-3-Benzyloxycarbonyl-5-(2-chloroethyl)-4-isobutyl-2,2-dimethyloxazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 116993-91-0
Methyl (4S,5S)-3-Benzyloxycarbonyl-5-(2-hydroxyethyl)-4-isobutyl-2,2-dimethyloxazolidine

: 98-59-9
p-toluenesulfonyl chloride

: 116993-92-1
(4S,5S)-3-Benzyloxycarbonyl-5-(2-chloroethyl)-4-isobutyl-2,2-dimethyloxazolidine

: 116993-93-2
(4S,5S)-3-benzyloxycarbonyl-2,2-dimethyl-5-(2-p-toluenesulfonyloxyethyl)-4-isobutyloxazolidine

Guidance literature:: With pyridine; Yield given; Ambient temperature;
DOI:10.1246/bcsj.63.2224

Reference yield:

: 49642-07-1
statine

: 116993-92-1
(4S,5S)-3-Benzyloxycarbonyl-5-(2-chloroethyl)-4-isobutyl-2,2-dimethyloxazolidine

Guidance literature:: Multi-step reaction with 5 steps

1: 93 percent / Et₃N / dioxane; H₂O / 30 °C

2: HCl / 1) r.t., 24h, 2) 40 deg C, 24h

3: 91 percent / p-toluenesulfonic acid / 1) r.t., 2h, 2) 38 deg C_., 1h

4: 99.7 percent / NaBH₄ / ethanol

5: pyridine / Ambient temperature

With pyridine; hydrogenchloride; sodium tetrahydroborate; toluene-4-sulfonic acid; triethylamine; In 1,4-dioxane; ethanol; water;
DOI:10.1246/bcsj.63.2224

Reference yield:

: 93287-37-7
(3S,4S)-4-(carbamic acid benzyl ester)-3-hydroxy-6-methyl-heptanoic acid

: 116993-92-1
(4S,5S)-3-Benzyloxycarbonyl-5-(2-chloroethyl)-4-isobutyl-2,2-dimethyloxazolidine

Guidance literature:: Multi-step reaction with 4 steps

1: HCl / 1) r.t., 24h, 2) 40 deg C, 24h

2: 91 percent / p-toluenesulfonic acid / 1) r.t., 2h, 2) 38 deg C_., 1h

3: 99.7 percent / NaBH₄ / ethanol

4: pyridine / Ambient temperature

With pyridine; hydrogenchloride; sodium tetrahydroborate; toluene-4-sulfonic acid; In ethanol;
DOI:10.1246/bcsj.63.2224