Methyl (4S,5S)-3-Benzyloxycarbonyl-5-(2-hydroxyethyl)-4-isobutyl-2,2-dimethyloxazolidine

Base Information

Chemical Name:Methyl (4S,5S)-3-Benzyloxycarbonyl-5-(2-hydroxyethyl)-4-isobutyl-2,2-dimethyloxazolidine
CAS No.:116993-91-0
Molecular Formula:C₁₉H₂₉NO₄
Molecular Weight:335.444
Hs Code.:

Synonyms:Methyl (4S,5S)-3-Benzyloxycarbonyl-5-(2-hydroxyethyl)-4-isobutyl-2,2-dimethyloxazolidine

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Chemical Property of Methyl (4S,5S)-3-Benzyloxycarbonyl-5-(2-hydroxyethyl)-4-isobutyl-2,2-dimethyloxazolidine

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Technology Process of Methyl (4S,5S)-3-Benzyloxycarbonyl-5-(2-hydroxyethyl)-4-isobutyl-2,2-dimethyloxazolidine

There total 5 articles about Methyl (4S,5S)-3-Benzyloxycarbonyl-5-(2-hydroxyethyl)-4-isobutyl-2,2-dimethyloxazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.7%

: 116993-90-9
Methyl <(4S,5S)-3-Benzyloxycarbonyl-4-isobutyl-2,2-dimethyl-5-oxazolidinyl> Acetate

: 116993-91-0
Methyl (4S,5S)-3-Benzyloxycarbonyl-5-(2-hydroxyethyl)-4-isobutyl-2,2-dimethyloxazolidine

Guidance literature:: With sodium tetrahydroborate; In ethanol;
DOI:10.1246/bcsj.63.2224

Reference yield:

: 49642-07-1
statine

: 116993-91-0
Methyl (4S,5S)-3-Benzyloxycarbonyl-5-(2-hydroxyethyl)-4-isobutyl-2,2-dimethyloxazolidine

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / Et₃N / dioxane; H₂O / 30 °C

2: HCl / 1) r.t., 24h, 2) 40 deg C, 24h

3: 91 percent / p-toluenesulfonic acid / 1) r.t., 2h, 2) 38 deg C_., 1h

4: 99.7 percent / NaBH₄ / ethanol

With hydrogenchloride; sodium tetrahydroborate; toluene-4-sulfonic acid; triethylamine; In 1,4-dioxane; ethanol; water;
DOI:10.1246/bcsj.63.2224

Reference yield:

: 93287-37-7
(3S,4S)-4-(carbamic acid benzyl ester)-3-hydroxy-6-methyl-heptanoic acid

: 116993-91-0
Methyl (4S,5S)-3-Benzyloxycarbonyl-5-(2-hydroxyethyl)-4-isobutyl-2,2-dimethyloxazolidine

Guidance literature:: Multi-step reaction with 3 steps

1: HCl / 1) r.t., 24h, 2) 40 deg C, 24h

2: 91 percent / p-toluenesulfonic acid / 1) r.t., 2h, 2) 38 deg C_., 1h

3: 99.7 percent / NaBH₄ / ethanol

With hydrogenchloride; sodium tetrahydroborate; toluene-4-sulfonic acid; In ethanol;
DOI:10.1246/bcsj.63.2224