(4S,5S)-3-Benzyloxycarbonyl-5-ethenyl-4-isobutyl-2,2-dimethyloxazolidine

Base Information

Chemical Name:(4S,5S)-3-Benzyloxycarbonyl-5-ethenyl-4-isobutyl-2,2-dimethyloxazolidine
CAS No.:116993-94-3
Molecular Formula:C₁₉H₂₇NO₃
Molecular Weight:317.428
Hs Code.:

Synonyms:(4S,5S)-3-Benzyloxycarbonyl-5-ethenyl-4-isobutyl-2,2-dimethyloxazolidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4S,5S)-3-Benzyloxycarbonyl-5-ethenyl-4-isobutyl-2,2-dimethyloxazolidine

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Technology Process of (4S,5S)-3-Benzyloxycarbonyl-5-ethenyl-4-isobutyl-2,2-dimethyloxazolidine

There total 11 articles about (4S,5S)-3-Benzyloxycarbonyl-5-ethenyl-4-isobutyl-2,2-dimethyloxazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 116993-92-1
(4S,5S)-3-Benzyloxycarbonyl-5-(2-chloroethyl)-4-isobutyl-2,2-dimethyloxazolidine

: 116993-94-3
(4S,5S)-3-Benzyloxycarbonyl-5-ethenyl-4-isobutyl-2,2-dimethyloxazolidine

Guidance literature:: With potassium tert-butylate; dimethyl sulfoxide; In benzene; for 0.166667h; Ambient temperature;
DOI:10.1246/bcsj.63.2224

Reference yield:

: C₁₆H₂₃NO₃

: 77-76-9
2,2-dimethoxy-propane

: 116993-94-3
(4S,5S)-3-Benzyloxycarbonyl-5-ethenyl-4-isobutyl-2,2-dimethyloxazolidine

Guidance literature:: With boron trifluoride diethyl etherate; In acetone; at 20 ℃; for 5h;
DOI:10.1016/j.bmc.2015.07.023

Reference yield:

: 49642-07-1
statine

: 116993-94-3
(4S,5S)-3-Benzyloxycarbonyl-5-ethenyl-4-isobutyl-2,2-dimethyloxazolidine

Guidance literature:: Multi-step reaction with 6 steps

1: 93 percent / Et₃N / dioxane; H₂O / 30 °C

2: HCl / 1) r.t., 24h, 2) 40 deg C, 24h

3: 91 percent / p-toluenesulfonic acid / 1) r.t., 2h, 2) 38 deg C_., 1h

4: 99.7 percent / NaBH₄ / ethanol

5: pyridine / Ambient temperature

6: 99 percent / t-BuOK, DMSO / benzene / 0.17 h / Ambient temperature

With pyridine; hydrogenchloride; sodium tetrahydroborate; potassium tert-butylate; toluene-4-sulfonic acid; dimethyl sulfoxide; triethylamine; In 1,4-dioxane; ethanol; water; benzene;
DOI:10.1246/bcsj.63.2224