trans-N-[4-(2-{4-[2-tert-butyl-6-(2-methoxyethyl)pyrimidin-4-yl]piperazin-1-yl}ethyl)cyclohexyl]formamide

Base Information

Chemical Name:trans-N-[4-(2-{4-[2-tert-butyl-6-(2-methoxyethyl)pyrimidin-4-yl]piperazin-1-yl}ethyl)cyclohexyl]formamide
CAS No.:1607474-54-3
Molecular Formula:C₂₄H₄₁N₅O₂
Molecular Weight:431.622
Hs Code.:

Synonyms:trans-N-[4-(2-{4-[2-tert-butyl-6-(2-methoxyethyl)pyrimidin-4-yl]piperazin-1-yl}ethyl)cyclohexyl]formamide

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Chemical Property of trans-N-[4-(2-{4-[2-tert-butyl-6-(2-methoxyethyl)pyrimidin-4-yl]piperazin-1-yl}ethyl)cyclohexyl]formamide

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Technology Process of trans-N-[4-(2-{4-[2-tert-butyl-6-(2-methoxyethyl)pyrimidin-4-yl]piperazin-1-yl}ethyl)cyclohexyl]formamide

There total 6 articles about trans-N-[4-(2-{4-[2-tert-butyl-6-(2-methoxyethyl)pyrimidin-4-yl]piperazin-1-yl}ethyl)cyclohexyl]formamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1607474-29-2
trans-4-(2-{4-[2-tert-butyl-6-(2-methoxyethyl)pyrimidin-4-yl]piperazin-1-yl}ethyl)cyclohexylamine

: 109-94-4
formic acid ethyl ester

: 1607474-54-3
trans-N-[4-(2-{4-[2-tert-butyl-6-(2-methoxyethyl)pyrimidin-4-yl]piperazin-1-yl}ethyl)cyclohexyl]formamide

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 3h;

Reference yield:

: 1607474-23-6
2-tert-butyl-4-(2-methoxyethyl)-6-piperazin-1-ylpyrimidine

: 1607474-54-3
trans-N-[4-(2-{4-[2-tert-butyl-6-(2-methoxyethyl)pyrimidin-4-yl]piperazin-1-yl}ethyl)cyclohexyl]formamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic acid / dichloromethane / 0.17 h / 20 °C

1.2: 4 h

2.1: hydrogenchloride / methanol; water / 16 h / 25 °C

3.1: triethylamine / dichloromethane / 3 h / 20 °C

With hydrogenchloride; acetic acid; triethylamine; In methanol; dichloromethane; water;

Reference yield:

: 1607474-28-1
trans-[4-(2-{4-[2-tert-butyl-6-(2-methoxyethyl)pyrimidin-4-yl]piperazin-1-yl}ethyl)cyclohexyl]carbamic acid tert-butyl ester

: 1607474-54-3
trans-N-[4-(2-{4-[2-tert-butyl-6-(2-methoxyethyl)pyrimidin-4-yl]piperazin-1-yl}ethyl)cyclohexyl]formamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / methanol; water / 16 h / 25 °C

2: triethylamine / dichloromethane / 3 h / 20 °C

With hydrogenchloride; triethylamine; In methanol; dichloromethane; water;