1-Methyl-2-[(2-methyl-5-nitrophenyl)methyl]-4-nitrobenzene

Base Information

• Chemical Name: 1-Methyl-2-[(2-methyl-5-nitrophenyl)methyl]-4-nitrobenzene
• CAS No.: 86409-50-9
• Molecular Formula: C₁₅H₁₄N₂O₄
• Molecular Weight: 286.287
• DSSTox Substance ID: DTXSID101265959

Synonyms:1-methyl-2-[(2-methyl-5-nitrophenyl)methyl]-4-nitrobenzene;SCHEMBL14768876;YCDBZNDEIDDULQ-UHFFFAOYSA-N;DTXSID101265959;86409-50-9;1,1'-Methylenebis[2-methyl-5-nitrobenzene]

Chemical Property of 1-Methyl-2-[(2-methyl-5-nitrophenyl)methyl]-4-nitrobenzene

Chemical Property:

• XLogP3: 4.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 2
• Exact Mass: 286.09535693
• Heavy Atom Count: 21
• Complexity: 354

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CC1=C(C=C(C=C1)[N+](=O)[O-])CC2=C(C=CC(=C2)[N+](=O)[O-])C

Technology Process of 1-Methyl-2-[(2-methyl-5-nitrophenyl)methyl]-4-nitrobenzene

There total 8 articles about 1-Methyl-2-[(2-methyl-5-nitrophenyl)methyl]-4-nitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

acetamide (60-35-5) + formaldehyd (50-00-0,30525-89-4,61233-19-0) + 1-methyl-4-nitrobenzene (99-99-0) → bis-(2-methyl-5-nitro-phenyl)-methane (86409-50-9) + N-(2-methyl-5-nitrobenzyl)acetamide (86392-53-2)

Guidance literature:

With conc. H₂SO₄; In sulfuric acid; at 55 ℃; for 8h; Product distribution; var. time, var. conc., var. temp.;

DOI:10.1021/jo00165a035

Reference yield: 65.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + 1-methyl-4-nitrobenzene (99-99-0) + N-(hydroxymethyl)acetamide (625-51-4) → bis-(2-methyl-5-nitro-phenyl)-methane (86409-50-9) + N-(2-methyl-5-nitrobenzyl)acetamide (86392-53-2)

Guidance literature:

In sulfuric acid; at 55 ℃; for 8h;

DOI:10.1021/jo00165a035

Reference yield: 43.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + 1-methyl-4-nitrobenzene (99-99-0) + N-(hydroxymethyl)benzamide (6282-02-6) → N-(2-methyl-5-nitrobenzyl)benzamide (86392-54-3) + bis-(2-methyl-5-nitro-phenyl)-methane (86409-50-9)

Guidance literature:

In sulfuric acid; for 168h; Ambient temperature;

DOI:10.1021/jo00165a035

upstream raw materials:

formaldehyd

1-methyl-4-nitrobenzene

bis(2-chloromethyl)ether

acetamide

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 86409-50-9 bis-(2-methyl-5-nitro-phenyl)-methane

Send

Send

Metric Ton KG G Pound L ML

Send

Send