(3R,4R)-4-methyl-1-phenylhex-5-en-3-ol?

Base Information

Chemical Name:(3R,4R)-4-methyl-1-phenylhex-5-en-3-ol?
CAS No.:129170-74-7
Molecular Formula:C₁₃H₁₈O
Molecular Weight:190.285
Hs Code.:

Synonyms:(3R,4R)-4-methyl-1-phenylhex-5-en-3-ol?

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3R,4R)-4-methyl-1-phenylhex-5-en-3-ol?

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Technology Process of (3R,4R)-4-methyl-1-phenylhex-5-en-3-ol?

There total 60 articles about (3R,4R)-4-methyl-1-phenylhex-5-en-3-ol? which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 104-53-0
3-phenyl-propionaldehyde

: 4894-61-5
trans-but-2-enyl chloride

: 83173-74-4,89103-73-1,89103-74-2,104011-57-6,106756-95-0,129170-74-7
(anti)-4-hydroxy-3-methyl-6-phenyl-1-hexene

: 104011-57-6
4-methyl-1-phenylhex-5-en-3-ol

Guidance literature:: With trichlorosilane; N-ethyl-N,N-diisopropylamine; copper(l) chloride; In diethyl ether; N,N-dimethyl-formamide; at 0 ℃; for 12h; Yield given;
DOI:10.1021/jo00101a021

Reference yield: 83.0%

: 104-53-0
3-phenyl-propionaldehyde

: 804559-38-4
(R,R)-crotylsilane

: 129170-74-7
(3R,4R)-4-methyl-1-phenylhex-5-en-3-ol?

Guidance literature:: With scandium tris(trifluoromethanesulfonate); In dichloromethane; at 0 ℃; for 3h; Inert atmosphere;
DOI:10.1021/ol3033237

Reference yield: 76.0%

: 104-53-0
3-phenyl-propionaldehyde

: 4784-77-4,39616-19-8,29576-14-5
(E)-1-Bromo-2-butene

: 83173-74-4,89103-73-1,104011-57-6,106756-95-0,129170-74-7,89103-74-2
(3S,4R)-3-methyl-6-phenyl-1-hexen-4-ol

Guidance literature:: (E)-1-Bromo-2-butene; With trichlorosilane; triethylamine; copper(I) bromide; In dichloromethane; at 0 ℃; for 2h; Inert atmosphere;

With 2-(tert-butyl)-6-((((1R,2R)-2-(methylamino)cyclohexyl)amino)methyl)phenol; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 0 - 23 ℃; for 1h; Inert atmosphere;

3-phenyl-propionaldehyde; enantioselective reaction; Further stages;
DOI:10.1021/acs.orglett.7b03193