N-(3,4-dimethoxy-6-cyanophenyl)-N',N'-(3-carboxamidopentamethylene)-S-methylisothiourea

Base Information

Chemical Name:N-(3,4-dimethoxy-6-cyanophenyl)-N',N'-(3-carboxamidopentamethylene)-S-methylisothiourea
CAS No.:80030-57-5
Molecular Formula:C₁₇H₂₂N₄O₃S
Molecular Weight:362.453
Hs Code.:

Synonyms:N-(3,4-dimethoxy-6-cyanophenyl)-N',N'-(3-carboxamidopentamethylene)-S-methylisothiourea

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(3,4-dimethoxy-6-cyanophenyl)-N',N'-(3-carboxamidopentamethylene)-S-methylisothiourea

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Technology Process of N-(3,4-dimethoxy-6-cyanophenyl)-N',N'-(3-carboxamidopentamethylene)-S-methylisothiourea

There total 3 articles about N-(3,4-dimethoxy-6-cyanophenyl)-N',N'-(3-carboxamidopentamethylene)-S-methylisothiourea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 86543-06-8
N-(3,4-dimethoxy-6-cyanophenyl)-N',N'-(3-carboxamidopentamethylene)thiourea

: 74-88-4
methyl iodide

: 80030-57-5
N-(3,4-dimethoxy-6-cyanophenyl)-N',N'-(3-carboxamidopentamethylene)-S-methylisothiourea

Guidance literature:: With calcium oxide; In chloroform; at 60 ℃; for 18h;
DOI:10.1021/jm00364a014

Reference yield:

: 39546-32-2
4-carboxamidopiperidine

: 80030-57-5
N-(3,4-dimethoxy-6-cyanophenyl)-N',N'-(3-carboxamidopentamethylene)-S-methylisothiourea

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / dimethylformamide / 20 h / 0 °C

2: 92 percent / calcium oxide / CHCl₃ / 18 h / 60 °C

With calcium oxide; In chloroform; N,N-dimethyl-formamide;
DOI:10.1021/jm00364a014

Reference yield:

: 43091-89-0
2-isothiocyanato-4,5-dimethoxybenzonitrile

: 80030-57-5
N-(3,4-dimethoxy-6-cyanophenyl)-N',N'-(3-carboxamidopentamethylene)-S-methylisothiourea

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / dimethylformamide / 20 h / 0 °C

2: 92 percent / calcium oxide / CHCl₃ / 18 h / 60 °C

With calcium oxide; In chloroform; N,N-dimethyl-formamide;
DOI:10.1021/jm00364a014