C₁₅H₂₀BrNO₃S

Base Information

Chemical Name:C₁₅H₂₀BrNO₃S
CAS No.:1352419-94-3
Molecular Formula:C₁₅H₂₀BrNO₃S
Molecular Weight:374.299
Hs Code.:

C<sub>15</sub>H<sub>20</sub>BrNO<sub>3</sub>S

Synonyms:C₁₅H₂₀BrNO₃S

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Chemical Property of C₁₅H₂₀BrNO₃S

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Technology Process of C₁₅H₂₀BrNO₃S

There total 1 articles about C₁₅H₂₀BrNO₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 546-68-9
titanium(IV) isopropylate

: 62123-80-2
ethyl 2-(3-bromo-phenyl)-2-oxo-acetate

: 343338-28-3
(S)-2-methylpropane-2-sulfinamide

: 1352419-94-3
C₁₅H₂₀BrNO₃S

Guidance literature:: In n-heptane; at 80 ℃; for 4h;

Reference yield: 99.0%

: 1352419-94-3
C₁₅H₂₀BrNO₃S

: 23719-80-4
cyclopropylmagnesium bromide

: 1352419-95-4
C₁₈H₂₆BrNO₃S

Guidance literature:: In dichloromethane; at -40 ℃; for 0.5h;

Reference yield:

: 1352419-94-3
C₁₅H₂₀BrNO₃S

: 1352420-02-0
C₁₄H₁₂BrF₄NOS

Guidance literature:: Multi-step reaction with 8 steps

1: dichloromethane / 0.5 h / -40 °C

2: sodium hydroxide / water; methanol / 4 h / Reflux

3: hydrogenchloride / 1,4-dioxane / 0.5 h / 20 °C

4: sodium hydroxide / water; tetrahydrofuran / 1 h / 15 °C / pH 10 - 11

5: sodium hydrogencarbonate / N,N-dimethyl-formamide / 2 h / 80 °C

6: tetrabutylammonium triphenyldifluorosilicate / tetrahydrofuran / 2 h / 20 °C

7: diethylamino-sulfur trifluoride / dichloromethane / 1 h / 20 °C

8: tetraphosphorus decasulfide / tetrahydrofuran / 3 h / 20 - 70 °C

With hydrogenchloride; tetraphosphorus decasulfide; diethylamino-sulfur trifluoride; sodium hydrogencarbonate; tetrabutylammonium triphenyldifluorosilicate; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide;