methoxo(4-(5-(1-aza-15-crown-5-1-yl))phenyl-10,15-diphenylsubporphyrinato)boron(III)

Base Information

Chemical Name:methoxo(4-(5-(1-aza-15-crown-5-1-yl))phenyl-10,15-diphenylsubporphyrinato)boron(III)
CAS No.:1057487-42-9
Molecular Formula:C₄₄H₄₃BN₄O₅
Molecular Weight:718.66
Hs Code.:

Synonyms:methoxo(4-(5-(1-aza-15-crown-5-1-yl))phenyl-10,15-diphenylsubporphyrinato)boron(III)

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Chemical Property of methoxo(4-(5-(1-aza-15-crown-5-1-yl))phenyl-10,15-diphenylsubporphyrinato)boron(III)

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Technology Process of methoxo(4-(5-(1-aza-15-crown-5-1-yl))phenyl-10,15-diphenylsubporphyrinato)boron(III)

There total 1 articles about methoxo(4-(5-(1-aza-15-crown-5-1-yl))phenyl-10,15-diphenylsubporphyrinato)boron(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 0.7%

: 67-56-1
methanol

: pyridine-tri(N-pyrrolyl)borane

: 100-52-7
benzaldehyde

: 1122-91-4
4-bromo-benzaldehyde

: 66943-05-3
1,4,7,10-tetraoxa-15-azacyclopentadecane

: 1057487-42-9
methoxo(4-(5-(1-aza-15-crown-5-1-yl))phenyl-10,15-diphenylsubporphyrinato)boron(III)

Guidance literature:: pyridine-tri(N-pyrrolyl)borane; benzaldehyde; 4-bromo-benzaldehyde; With trifluoroacetic acid; In 1,2-dichloro-benzene; at 0 ℃; for 0.5h; Inert atmosphere;

With pyridine; In 1,2-dichloro-benzene; for 1h; Reflux;

methanol; 1,4,7,10-tetraoxa-15-azacyclopentadecane; Further stages;
DOI:10.1021/ja804846v