N-methyl-9H-fluoren-2-amine

Base Information

Chemical Name:N-methyl-9H-fluoren-2-amine
CAS No.:63019-68-1
Molecular Formula:C14H13N
Molecular Weight:195.264
Hs Code.:2921499090
Mol file:63019-68-1.mol

Synonyms:2-Methylamino-fluoren;2-Fluorenylmonomethylamine;N-Methyl-fluorenamin-(2);2-Monomethylaminofluorene;fluoren-2-yl-methyl-amine;N-Methyl-2-fluorenamin;N-Monomethyl-2-aminofluorene;2-Methylaminofluorene;FLUOREN-2-AMINE,N-METHYL;

Suppliers and Price of N-methyl-9H-fluoren-2-amine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 5 raw suppliers

Chemical Property of N-methyl-9H-fluoren-2-amine

Chemical Property:

Vapor Pressure:7.73E-06mmHg at 25°C
Melting Point:78-78.5 °C(Solv: cyclopentane (287-92-3))
Refractive Index:1.6353 (estimate)
Boiling Point:375.5°C at 760 mmHg
PKA:4.88±0.20(Predicted)
Flash Point:197.8°C
PSA：12.03000
Density:1.163g/cm³
LogP:3.37250

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of N-methyl-9H-fluoren-2-amine

There total 10 articles about N-methyl-9H-fluoren-2-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 67-56-1
methanol

: 153-78-6
2-aminofluorene

: 63019-68-1
N-methyl-9H-fluoren-2-amine

Guidance literature:: With dimanganese decacarbonyl; potassium tert-butylate; In toluene; at 100 ℃; for 24h; Inert atmosphere; Sealed tube;
DOI:10.1039/c9cc02989c

Reference yield:

: C₁₄H₁₁N

: 63019-68-1
N-methyl-9H-fluoren-2-amine

Guidance literature:: With sodium tetrahydroborate; at 0 ℃; for 2h; Reflux;
DOI:10.1021/acs.orglett.6b03458

Reference yield:

: 153-78-6
2-aminofluorene

: 63019-68-1
N-methyl-9H-fluoren-2-amine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium / methanol / 2 h / 0 °C / Reflux

2: sodium tetrahydroborate / 2 h / 0 °C / Reflux

With sodium tetrahydroborate; sodium; In methanol;
DOI:10.1021/acs.orglett.6b03458