1,1'-[1,3-bis(cyclohexyl)hexahydropyrimidine-5,5-diyl]diethanone

Base Information

• Chemical Name: 1,1'-[1,3-bis(cyclohexyl)hexahydropyrimidine-5,5-diyl]diethanone
• CAS No.: 1620088-76-7
• Molecular Formula: C₂₀H₃₄N₂O₂
• Molecular Weight: 334.502
• Mol file: 1620088-76-7.mol

Synonyms:1,1'-[1,3-bis(cyclohexyl)hexahydropyrimidine-5,5-diyl]diethanone

Chemical Property of 1,1'-[1,3-bis(cyclohexyl)hexahydropyrimidine-5,5-diyl]diethanone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,1'-[1,3-bis(cyclohexyl)hexahydropyrimidine-5,5-diyl]diethanone

There total 1 articles about 1,1'-[1,3-bis(cyclohexyl)hexahydropyrimidine-5,5-diyl]diethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + cyclohexylamine (108-91-8,157973-60-9) + acetylacetone (123-54-6,81235-32-7) → 1,1'-[1,3-bis(cyclohexyl)hexahydropyrimidine-5,5-diyl]diethanone (1620088-76-7)

Guidance literature:

With iron(III) chloride; In dichloromethane; water; at 20 ℃; for 24h;

DOI:10.1080/00397911.2014.916302

Reference yield: 75.0%

1,1'-[1,3-bis(cyclohexyl)hexahydropyrimidine-5,5-diyl]diethanone (1620088-76-7) → C12H21N3

Guidance literature:

With hydrazine hydrate; In ethanol; at 20 ℃; for 24h;

DOI:10.1515/chempap-2015-0018

upstream raw materials:

formaldehyd

cyclohexylamine

acetylacetone