N-(9-fluorenylmethoxycarbonyl)-O-[(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3-di-O-(4-methylbenzoyl)-β-D-xylopyranosyl]-L-serylglycine

Base Information

Chemical Name:N-(9-fluorenylmethoxycarbonyl)-O-[(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3-di-O-(4-methylbenzoyl)-β-D-xylopyranosyl]-L-serylglycine
CAS No.:1254303-65-5
Molecular Formula:C₇₈H₈₈N₂O₃₇
Molecular Weight:1645.55
Hs Code.:

N-(9-fluorenylmethoxycarbonyl)-O-[(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3-di-O-(4-methylbenzoyl)-β-D-xylopyranosyl]-L-serylglycine

Synonyms:N-(9-fluorenylmethoxycarbonyl)-O-[(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3-di-O-(4-methylbenzoyl)-β-D-xylopyranosyl]-L-serylglycine

Suppliers and Price of N-(9-fluorenylmethoxycarbonyl)-O-[(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3-di-O-(4-methylbenzoyl)-β-D-xylopyranosyl]-L-serylglycine

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Chemical Property of N-(9-fluorenylmethoxycarbonyl)-O-[(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3-di-O-(4-methylbenzoyl)-β-D-xylopyranosyl]-L-serylglycine

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Technology Process of N-(9-fluorenylmethoxycarbonyl)-O-[(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3-di-O-(4-methylbenzoyl)-β-D-xylopyranosyl]-L-serylglycine

There total 1 articles about N-(9-fluorenylmethoxycarbonyl)-O-[(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3-di-O-(4-methylbenzoyl)-β-D-xylopyranosyl]-L-serylglycine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1254303-64-4
N-(9-fluorenylmethoxycarbonyl)-O-[(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3-di-O-(4-methylbenzoyl)-β-D-xylopyranosyl]-L-serylglycine allyl ester

: 1254303-65-5
N-(9-fluorenylmethoxycarbonyl)-O-[(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3-di-O-(4-methylbenzoyl)-β-D-xylopyranosyl]-L-serylglycine

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; N-methylaniline; In tetrahydrofuran; for 2h; Inert atmosphere;
DOI:10.1016/j.carres.2010.06.019

Reference yield:

: 1254303-68-8
O-(tert-butyl)-L-aspartyl-L-asparaginylglycine methyl ester

: 1254303-65-5
N-(9-fluorenylmethoxycarbonyl)-O-[(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3-di-O-(4-methylbenzoyl)-β-D-xylopyranosyl]-L-serylglycine

: C₉₃H₁₁₂N₆O₄₃

Guidance literature:: N-(9-fluorenylmethoxycarbonyl)-O-[(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3-di-O-(4-methylbenzoyl)-β-D-xylopyranosyl]-L-serylglycine; With benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; In N,N-dimethyl-formamide; at -20 - 20 ℃; Inert atmosphere;

O-(tert-butyl)-L-aspartyl-L-asparaginylglycine methyl ester; With N-ethyl-N,N-diisopropylamine; Inert atmosphere;
DOI:10.1016/j.carres.2010.06.019

Reference yield:

: Fmoc-Sieber amide resin

: 1254303-65-5
N-(9-fluorenylmethoxycarbonyl)-O-[(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3-di-O-(4-methylbenzoyl)-β-D-xylopyranosyl]-L-serylglycine

: 29022-11-5
N-(fluoren-9-ylmethoxycarbonyl)glycine

: 71989-31-6
Fmoc-Pro-OH

: 35661-40-6
N-Fmoc L-Phe

: 71989-14-5
Fmoc-(tBu)Asp-OH

: 132388-59-1
L-Asn(Trt)

: C₈₉H₁₁₂N₁₀O₄₅

Guidance literature:: Fmoc-Sieber amide resin; With piperidine; In 1-methyl-pyrrolidin-2-one; solid phase reaction;

N-(fluoren-9-ylmethoxycarbonyl)glycine; With benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In 1-methyl-pyrrolidin-2-one; solid phase reaction;

N-(9-fluorenylmethoxycarbonyl)-O-[(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->3)-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-(1->4)-2,3-di-O-(4-methylbenzoyl)-β-D-xylopyranosyl]-L-serylglycine; Fmoc-Pro-OH; N-Fmoc L-Phe; Fmoc-(tBu)Asp-OH; L-Asn(Trt); Further stages;
DOI:10.1016/j.carres.2010.06.019