(2S,4S)-(+)-2-<(4S,5S)-(2,2-Dimethyl-4-phenyl-1,3-dioxan-5-yl)amino>-5,5,5-trifluor-4-methylvaleronitril

Base Information

Chemical Name:(2S,4S)-(+)-2-<(4S,5S)-(2,2-Dimethyl-4-phenyl-1,3-dioxan-5-yl)amino>-5,5,5-trifluor-4-methylvaleronitril
CAS No.:95911-00-5
Molecular Formula:C₁₈H₂₃F₃N₂O₂
Molecular Weight:356.388
Hs Code.:

Synonyms:(2S,4S)-(+)-2-<(4S,5S)-(2,2-Dimethyl-4-phenyl-1,3-dioxan-5-yl)amino>-5,5,5-trifluor-4-methylvaleronitril

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Chemical Property of (2S,4S)-(+)-2-<(4S,5S)-(2,2-Dimethyl-4-phenyl-1,3-dioxan-5-yl)amino>-5,5,5-trifluor-4-methylvaleronitril

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Technology Process of (2S,4S)-(+)-2-<(4S,5S)-(2,2-Dimethyl-4-phenyl-1,3-dioxan-5-yl)amino>-5,5,5-trifluor-4-methylvaleronitril

There total 6 articles about (2S,4S)-(+)-2-<(4S,5S)-(2,2-Dimethyl-4-phenyl-1,3-dioxan-5-yl)amino>-5,5,5-trifluor-4-methylvaleronitril which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 691-77-0
(E)-3-trifluoromethyl-2-butenoic acid ethyl ester

: 95853-76-2,95911-00-5,95911-01-6,95976-40-2
(2S,4R)-(+)-2-<(4S,5S)-(2,2-Dimethyl-4-phenyl-1,3-dioxan-5-yl)amino>-5,5,5-trifluor-4-methylvaleronitril

Guidance literature:: Multi-step reaction with 4 steps

1: 98 percent / H₂ / Pd/C (10 percent Pd) / 6 h / Ambient temperature

2: 74 percent / LiAlH₄ / diethyl ether / 2 h

3: 80 percent / PCC / CH₂Cl₂ / 1.5 h / Ambient temperature

4: ethane-1,2-diol / 0.25 h / Heating

With lithium aluminium tetrahydride; hydrogen; pyridinium chlorochromate; 10% palladium on active carbon; In diethyl ether; dichloromethane; ethylene glycol;

Reference yield:

: 6975-13-9
(+/-)-ethyl 4,4,4-trifluoro-3-methylbutanoate

: 95853-76-2,95911-00-5,95911-01-6,95976-40-2
(2S,4R)-(+)-2-<(4S,5S)-(2,2-Dimethyl-4-phenyl-1,3-dioxan-5-yl)amino>-5,5,5-trifluor-4-methylvaleronitril

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / LiAlH₄ / diethyl ether / 2 h

2: 80 percent / PCC / CH₂Cl₂ / 1.5 h / Ambient temperature

3: ethane-1,2-diol / 0.25 h / Heating

With lithium aluminium tetrahydride; pyridinium chlorochromate; In diethyl ether; dichloromethane; ethylene glycol;

Reference yield:

: 85571-88-6
(R)-(+)-4,4,4-Trifluor-3-methyl-1-butanol

: 95853-76-2,95911-00-5,95911-01-6,95976-40-2
(2S,4R)-(+)-2-<(4S,5S)-(2,2-Dimethyl-4-phenyl-1,3-dioxan-5-yl)amino>-5,5,5-trifluor-4-methylvaleronitril

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / PCC / CH₂Cl₂ / 1.5 h / Ambient temperature

2: ethane-1,2-diol / 0.25 h / Heating

With pyridinium chlorochromate; In dichloromethane; ethylene glycol;