Technology Process of C17H14BrF2NO2S
There total 4 articles about C17H14BrF2NO2S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dipotassium hydrogenphosphate; tris(bipyridine)ruthenium(II) dichloride hexahydrate;
In
dichloromethane;
at 40 ℃;
for 48h;
Sealed tube;
Inert atmosphere;
Irradiation;
DOI:10.1021/ol501094z
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 - 20 °C / Inert atmosphere
1.2: 0 - 20 °C / Inert atmosphere
2.1: tris(bipyridine)ruthenium(II) dichloride hexahydrate; dipotassium hydrogenphosphate / dichloromethane / 48 h / 40 °C / Sealed tube; Inert atmosphere; Irradiation
With
dipotassium hydrogenphosphate; tris(bipyridine)ruthenium(II) dichloride hexahydrate; sodium hydride;
In
dichloromethane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/ol501094z
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: zinc(II) chloride / para-xylene / 160 °C
2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 - 20 °C / Inert atmosphere
2.2: 0 - 20 °C / Inert atmosphere
3.1: tris(bipyridine)ruthenium(II) dichloride hexahydrate; dipotassium hydrogenphosphate / dichloromethane / 48 h / 40 °C / Sealed tube; Inert atmosphere; Irradiation
With
dipotassium hydrogenphosphate; tris(bipyridine)ruthenium(II) dichloride hexahydrate; sodium hydride; zinc(II) chloride;
In
dichloromethane; para-xylene; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/ol501094z
