2-[2-(1-methyl-2-piperidinyl)ethyl]-benzenamine 4-methylbenzenesulfonate

Base Information

Chemical Name:2-[2-(1-methyl-2-piperidinyl)ethyl]-benzenamine 4-methylbenzenesulfonate
CAS No.:951155-19-4
Molecular Formula:C₇H₈O₃S*C₁₄H₂₂N₂
Molecular Weight:390.547
Hs Code.:

Synonyms:2-[2-(1-methyl-2-piperidinyl)ethyl]-benzenamine 4-methylbenzenesulfonate

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Chemical Property of 2-[2-(1-methyl-2-piperidinyl)ethyl]-benzenamine 4-methylbenzenesulfonate

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Technology Process of 2-[2-(1-methyl-2-piperidinyl)ethyl]-benzenamine 4-methylbenzenesulfonate

There total 4 articles about 2-[2-(1-methyl-2-piperidinyl)ethyl]-benzenamine 4-methylbenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 951238-66-7
1-methyl-2-[(E)-2-(2-nitrophenyl)-ethenyl]-pyridinium 4-methylbenzenesulfonate

: 951155-19-4
2-[2-(1-methyl-2-piperidinyl)ethyl]-benzenamine 4-methylbenzenesulfonate

Guidance literature:: With 10% Pt/activated carbon; hydrogen; In methanol; at 30 ℃; under 749.884 - 3878.71 Torr; Inert atmosphere; Industrial scale;
DOI:10.1021/op5003402

Reference yield:

: 552-89-6
2-nitro-benzaldehyde

: 951155-19-4
2-[2-(1-methyl-2-piperidinyl)ethyl]-benzenamine 4-methylbenzenesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: acetic anhydride / 28 h / 140 °C / Industrial scale

2: acetonitrile / 24 h / 82 °C / Industrial scale

3: hydrogen; 10% Pt/activated carbon / methanol / 30 °C / 749.88 - 3878.71 Torr / Inert atmosphere; Industrial scale

With 10% Pt/activated carbon; hydrogen; In methanol; acetic anhydride; acetonitrile;
DOI:10.1021/op5003402

Reference yield:

: 109-06-8
α-picoline

: 951155-19-4
2-[2-(1-methyl-2-piperidinyl)ethyl]-benzenamine 4-methylbenzenesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: acetic anhydride / 28 h / 140 °C / Industrial scale

2: acetonitrile / 24 h / 82 °C / Industrial scale

3: hydrogen; 10% Pt/activated carbon / methanol / 30 °C / 749.88 - 3878.71 Torr / Inert atmosphere; Industrial scale

With 10% Pt/activated carbon; hydrogen; In methanol; acetic anhydride; acetonitrile;
DOI:10.1021/op5003402