tris[2-(diphenylphosphino)ethyl]methane

Base Information

Chemical Name:tris[2-(diphenylphosphino)ethyl]methane
CAS No.:175079-23-9
Molecular Formula:C₄₃H₄₃P₃
Molecular Weight:652.736
Hs Code.:

Synonyms:tris[2-(diphenylphosphino)ethyl]methane

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Chemical Property of tris[2-(diphenylphosphino)ethyl]methane

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Technology Process of tris[2-(diphenylphosphino)ethyl]methane

There total 1 articles about tris[2-(diphenylphosphino)ethyl]methane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 829-85-6
diphenylphosphane

: 134380-91-9
3-(2-chloroethyl)-1,5-dichloropentane

: 175079-23-9
tris[2-(diphenylphosphino)ethyl]methane

Guidance literature:: diphenylphosphane; With n-butyllithium; In tetrahydrofuran; hexane; at 0 ℃; for 1h; Inert atmosphere;

3-(2-chloroethyl)-1,5-dichloropentane; In tetrahydrofuran; hexane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/om200718j

Reference yield: 85.0%

: 15529-49-4,41756-81-4
tris(triphenylphosphine)ruthenium(II) chloride

: 75-09-2
dichloromethane

: 175079-23-9
tris[2-(diphenylphosphino)ethyl]methane

: [RuCl₂(tris[2-(diphenylphosphino)ethyl]methane)]4*dichloromethane

Guidance literature:: In dichloromethane; (inert atm.); keeping a soln. of Ru complex and ligand in CH2Cl2 at roomtemp. for 10 d; drying ppt. in vac.; elem. anal.;
DOI:10.1021/om200718j

Reference yield: 48.0%

: 15529-49-4,41756-81-4
tris(triphenylphosphine)ruthenium(II) chloride

: 175079-23-9
tris[2-(diphenylphosphino)ethyl]methane

: [Ru(C(CH₂CH₂PPh₂)2(=CHCH₂PPh₂))Cl₂]

Guidance literature:: In 1,3,5-trimethyl-benzene; (inert atm.); refluxing a mixt. of Ru complex and ligand in mesitylene for 18 h, cooling; filtration, washing ppt. with mesitylene, pentane, drying in vac.; elem.anal.;
DOI:10.1021/om200718j