4-(2-Benzyloxycarbamoyl-ethyl)-4-nitro-heptanedioic acid bis-(benzyloxy-amide)

Base Information

Chemical Name:4-(2-Benzyloxycarbamoyl-ethyl)-4-nitro-heptanedioic acid bis-(benzyloxy-amide)
CAS No.:141621-27-4
Molecular Formula:C₃₁H₃₆N₄O₈
Molecular Weight:592.649
Hs Code.:

Synonyms:4-(2-Benzyloxycarbamoyl-ethyl)-4-nitro-heptanedioic acid bis-(benzyloxy-amide)

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Chemical Property of 4-(2-Benzyloxycarbamoyl-ethyl)-4-nitro-heptanedioic acid bis-(benzyloxy-amide)

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Technology Process of 4-(2-Benzyloxycarbamoyl-ethyl)-4-nitro-heptanedioic acid bis-(benzyloxy-amide)

There total 4 articles about 4-(2-Benzyloxycarbamoyl-ethyl)-4-nitro-heptanedioic acid bis-(benzyloxy-amide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 59085-15-3
4-(2-carboxyethyl)-4-nitroheptanedioic acid

: 2687-43-6
O-benzylhydoxylamine hydrochloride

: 141621-27-4
4-(2-Benzyloxycarbamoyl-ethyl)-4-nitro-heptanedioic acid bis-(benzyloxy-amide)

Guidance literature:: With N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In tetrahydrofuran; water; Ambient temperature; pH ca. 4.8;
DOI:10.1016/S0040-4039(00)74153-0

Reference yield:

: 83935-54-0
dimethyl 4-nitro-4-<1-<2-(methoxycarbonyl)ethyl>>heptanedioate

: 141621-27-4
4-(2-Benzyloxycarbamoyl-ethyl)-4-nitro-heptanedioic acid bis-(benzyloxy-amide)

Guidance literature:: Multi-step reaction with 3 steps

1: 65 percent / NaOH / methanol / Heating

2: SOCl₂ / Heating

3: Et₃N / tetrahydrofuran / Ambient temperature

With sodium hydroxide; thionyl chloride; triethylamine; In tetrahydrofuran; methanol;
DOI:10.1039/a700300e

Reference yield:

: 59085-15-3
4-(2-carboxyethyl)-4-nitroheptanedioic acid

: 141621-27-4
4-(2-Benzyloxycarbamoyl-ethyl)-4-nitro-heptanedioic acid bis-(benzyloxy-amide)

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / Heating

2: Et₃N / tetrahydrofuran / Ambient temperature

With thionyl chloride; triethylamine; In tetrahydrofuran;
DOI:10.1039/a700300e