3-(t-butyldiphenylsilyl)oxymethyl-N-methoxy-N-methylpena-3,4-dienamide

Base Information

Chemical Name:3-(t-butyldiphenylsilyl)oxymethyl-N-methoxy-N-methylpena-3,4-dienamide
CAS No.:1434003-12-9
Molecular Formula:C₂₄H₃₁NO₃Si
Molecular Weight:409.601
Hs Code.:

Synonyms:3-(t-butyldiphenylsilyl)oxymethyl-N-methoxy-N-methylpena-3,4-dienamide

Suppliers and Price of 3-(t-butyldiphenylsilyl)oxymethyl-N-methoxy-N-methylpena-3,4-dienamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(t-butyldiphenylsilyl)oxymethyl-N-methoxy-N-methylpena-3,4-dienamide

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Technology Process of 3-(t-butyldiphenylsilyl)oxymethyl-N-methoxy-N-methylpena-3,4-dienamide

There total 2 articles about 3-(t-butyldiphenylsilyl)oxymethyl-N-methoxy-N-methylpena-3,4-dienamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1434003-11-8
ethyl 3-(((tert-butyldiphenylsilyl)oxy)methyl)penta-3,4-dienoate

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 1434003-12-9
3-(t-butyldiphenylsilyl)oxymethyl-N-methoxy-N-methylpena-3,4-dienamide

Guidance literature:: With isopropylmagnesium chloride; at -20 - -10 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ol400904y

Reference yield:

: 92808-80-5
4-((tert-butyldiphenylsilyl)oxy)but-2-yn-1-ol

: 1434003-12-9
3-(t-butyldiphenylsilyl)oxymethyl-N-methoxy-N-methylpena-3,4-dienamide

Guidance literature:: Multi-step reaction with 2 steps

1: propionic acid / 5 h / 130 °C / Inert atmosphere

2: isopropylmagnesium chloride / 2 h / -20 - -10 °C / Inert atmosphere

With isopropylmagnesium chloride; In propionic acid;
DOI:10.1021/ol400904y