methyl 4-O-(4-methoxybenzyl)-2,3-di-O-tetradecyl-α-D-gluco-hexodialdo-1,5-pyranose-6-O-methyloxime

Base Information

Chemical Name:methyl 4-O-(4-methoxybenzyl)-2,3-di-O-tetradecyl-α-D-gluco-hexodialdo-1,5-pyranose-6-O-methyloxime
CAS No.:872677-66-2
Molecular Formula:C₄₄H₇₉NO₇
Molecular Weight:734.114
Hs Code.:

Synonyms:methyl 4-O-(4-methoxybenzyl)-2,3-di-O-tetradecyl-α-D-gluco-hexodialdo-1,5-pyranose-6-O-methyloxime

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Chemical Property of methyl 4-O-(4-methoxybenzyl)-2,3-di-O-tetradecyl-α-D-gluco-hexodialdo-1,5-pyranose-6-O-methyloxime

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Technology Process of methyl 4-O-(4-methoxybenzyl)-2,3-di-O-tetradecyl-α-D-gluco-hexodialdo-1,5-pyranose-6-O-methyloxime

There total 8 articles about methyl 4-O-(4-methoxybenzyl)-2,3-di-O-tetradecyl-α-D-gluco-hexodialdo-1,5-pyranose-6-O-methyloxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 872677-65-1
methyl 4-O-(4-methoxybenzyl)-2,3-di-O-tetradecyl-α-D-gluco-hexodialdo-1,5-pyranoside

: 593-56-6
N-methoxylamine hydrochloride

: 872677-66-2
methyl 4-O-(4-methoxybenzyl)-2,3-di-O-tetradecyl-α-D-gluco-hexodialdo-1,5-pyranose-6-O-methyloxime

Guidance literature:: With pyridine; for 1.5h;

Reference yield:

: 637774-19-7
methyl 4-O-(4-methoxybenzyl)-2,3-di-O-tetradecyl-α-D-glucopyranoside

: 872677-66-2
methyl 4-O-(4-methoxybenzyl)-2,3-di-O-tetradecyl-α-D-gluco-hexodialdo-1,5-pyranose-6-O-methyloxime

Guidance literature:: Multi-step reaction with 2 steps

1: Dess-Martin periodinane / CH₂Cl₂ / 1 h

2: 540 mg / pyridine / 1.5 h

With pyridine; Dess-Martin periodane; In dichloromethane;
DOI:10.1016/j.bmc.2005.08.047

Reference yield:

: 637774-18-6
methyl 4,6-O-(4-methoxybenzylidene)-2,3-di-O-tetradecyl-α-D-glucopyranoside

: 872677-66-2
methyl 4-O-(4-methoxybenzyl)-2,3-di-O-tetradecyl-α-D-gluco-hexodialdo-1,5-pyranose-6-O-methyloxime

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / LiAlH₄; AlCl₃ / tetrahydrofuran; diethyl ether; CH₂Cl₂ / 4 h / Heating

2: Dess-Martin periodinane / CH₂Cl₂ / 1 h

3: 540 mg / pyridine / 1.5 h

With pyridine; lithium aluminium tetrahydride; aluminium trichloride; Dess-Martin periodane; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1016/j.bmc.2005.08.047