methyl 6-methoxyamino-4-O-(4-methoxybenzyl)-2,3-di-O-tetradecyl-6-deoxy-α-D-glucopyranoside

Base Information

Chemical Name:methyl 6-methoxyamino-4-O-(4-methoxybenzyl)-2,3-di-O-tetradecyl-6-deoxy-α-D-glucopyranoside
CAS No.:872677-67-3
Molecular Formula:C₄₄H₈₁NO₇
Molecular Weight:736.13
Hs Code.:

Synonyms:methyl 6-methoxyamino-4-O-(4-methoxybenzyl)-2,3-di-O-tetradecyl-6-deoxy-α-D-glucopyranoside

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Chemical Property of methyl 6-methoxyamino-4-O-(4-methoxybenzyl)-2,3-di-O-tetradecyl-6-deoxy-α-D-glucopyranoside

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Technology Process of methyl 6-methoxyamino-4-O-(4-methoxybenzyl)-2,3-di-O-tetradecyl-6-deoxy-α-D-glucopyranoside

There total 9 articles about methyl 6-methoxyamino-4-O-(4-methoxybenzyl)-2,3-di-O-tetradecyl-6-deoxy-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 872677-66-2
methyl 4-O-(4-methoxybenzyl)-2,3-di-O-tetradecyl-α-D-gluco-hexodialdo-1,5-pyranose-6-O-methyloxime

: 872677-67-3
methyl 6-methoxyamino-4-O-(4-methoxybenzyl)-2,3-di-O-tetradecyl-6-deoxy-α-D-glucopyranoside

Guidance literature:: With sodium cyanoborohydride; acetic acid; for 4h;
DOI:10.1016/j.bmc.2005.08.047

Reference yield:

: 637774-19-7
methyl 4-O-(4-methoxybenzyl)-2,3-di-O-tetradecyl-α-D-glucopyranoside

: 872677-67-3
methyl 6-methoxyamino-4-O-(4-methoxybenzyl)-2,3-di-O-tetradecyl-6-deoxy-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: Dess-Martin periodinane / CH₂Cl₂ / 1 h

2: 540 mg / pyridine / 1.5 h

3: 92 percent / sodium cyanoborohydride; acetic acid / 4 h

With pyridine; sodium cyanoborohydride; Dess-Martin periodane; acetic acid; In dichloromethane;
DOI:10.1016/j.bmc.2005.08.047

Reference yield:

: 637774-18-6
methyl 4,6-O-(4-methoxybenzylidene)-2,3-di-O-tetradecyl-α-D-glucopyranoside

: 872677-67-3
methyl 6-methoxyamino-4-O-(4-methoxybenzyl)-2,3-di-O-tetradecyl-6-deoxy-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 86 percent / LiAlH₄; AlCl₃ / tetrahydrofuran; diethyl ether; CH₂Cl₂ / 4 h / Heating

2: Dess-Martin periodinane / CH₂Cl₂ / 1 h

3: 540 mg / pyridine / 1.5 h

4: 92 percent / sodium cyanoborohydride; acetic acid / 4 h

With pyridine; lithium aluminium tetrahydride; aluminium trichloride; sodium cyanoborohydride; Dess-Martin periodane; acetic acid; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1016/j.bmc.2005.08.047