C₂₅H₂₆BrF₃N₂O₃S

Base Information

Chemical Name:C₂₅H₂₆BrF₃N₂O₃S
CAS No.:865234-99-7
Molecular Formula:C₂₅H₂₆BrF₃N₂O₃S
Molecular Weight:571.458
Hs Code.:

C<sub>25</sub>H<sub>26</sub>BrF<sub>3</sub>N<sub>2</sub>O<sub>3</sub>S

Synonyms:C₂₅H₂₆BrF₃N₂O₃S

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Chemical Property of C₂₅H₂₆BrF₃N₂O₃S

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Technology Process of C₂₅H₂₆BrF₃N₂O₃S

There total 6 articles about C₂₅H₂₆BrF₃N₂O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: C₂₂H₁₉BrF₃NO₃S

: 124-40-3
dimethyl amine

: 865234-99-7
C₂₅H₂₆BrF₃N₂O₃S

Guidance literature:: formaldehyd; C₂₂H₁₉BrF₃NO₃S; dimethyl amine; With acetic acid; In water; at 50 - 55 ℃; for 6 - 8h;

With sodium hydroxide; In water; pH=10;

Reference yield:

: 141-97-9
ethyl acetoacetate

: 865234-99-7
C₂₅H₂₆BrF₃N₂O₃S

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydroxide / diethyl ether; water / 17 h / 20 - 40 °C

1.2: pH 8

2.1: 1,2-dichloro-ethane / 8 h / 60 °C / Heating / reflux

3.1: pyridine / acetone / 4 h / 20 - 30 °C

4.1: bromine / dibenzoyl peroxide / tetrachloromethane / 5 h / Heating / reflux

5.1: potassium hydroxide / methanol / 2 h / 20 °C

5.2: 6 - 8 h / 20 °C

6.1: acetic acid / water / 6 - 8 h / 50 - 55 °C

6.2: pH 10

With pyridine; potassium hydroxide; sodium hydroxide; bromine; acetic acid; dibenzoyl peroxide; In methanol; tetrachloromethane; diethyl ether; water; 1,2-dichloro-ethane; acetone;

Reference yield:

: 383402-59-3
5-acetoxy-1-cyclopropyl-2-methyl-1H-indole-3-carboxylic acid ethyl ester

: 865234-99-7
C₂₅H₂₆BrF₃N₂O₃S

Guidance literature:: Multi-step reaction with 3 steps

1.1: bromine / dibenzoyl peroxide / tetrachloromethane / 5 h / Heating / reflux

2.1: potassium hydroxide / methanol / 2 h / 20 °C

2.2: 6 - 8 h / 20 °C

3.1: acetic acid / water / 6 - 8 h / 50 - 55 °C

3.2: pH 10

With potassium hydroxide; bromine; acetic acid; dibenzoyl peroxide; In methanol; tetrachloromethane; water;