4-Hydroxy-3-methoxy-benzaldehyde O-Methyloxime

Base Information

• Chemical Name: 4-Hydroxy-3-methoxy-benzaldehyde O-Methyloxime
• CAS No.: 93249-67-3
• Molecular Formula: C9H11 N O3
• Molecular Weight: 181.191
• Hs Code.: 2928000090
• Mol file: 93249-67-3.mol

Synonyms:4-Hydroxy-3-methoxy-benzaldehyde O-Methyloxime

Chemical Property of 4-Hydroxy-3-methoxy-benzaldehyde O-Methyloxime

Chemical Property:

• Vapor Pressure: 0.00332mmHg at 25°C
• Melting Point: NA
• Boiling Point: 282.6°Cat760mmHg
• Flash Point: 124.7°C
• PSA: 51.05000
• Density: 1.16g/cm³
• LogP: 1.38110
• Storage Temp.: Refrigerator
• Solubility.: Dichloromethane, Methanol

Purity/Quality:

98%Min ^*data from raw suppliers

4-Hydroxy-3-methoxybenzaldehydeO-Methyloxime ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: Capsaicin intermediate, as a possible carcinogen.

Technology Process of 4-Hydroxy-3-methoxy-benzaldehyde O-Methyloxime

There total 1 articles about 4-Hydroxy-3-methoxy-benzaldehyde O-Methyloxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

N-methoxylamine hydrochloride (593-56-6) + vanillin (121-33-5,8014-42-4) → 4-hydroxy-3-methoxybenzaldehyde O-methyloxime (93249-67-3)

Guidance literature:

With pyridine; Ambient temperature;

DOI:10.1021/jo00240a024

Reference yield:

4-hydroxy-3-methoxybenzaldehyde O-methyloxime (93249-67-3) → vanillylamine hydrochloride (7149-10-2)

Guidance literature:

With hydrogenchloride; hydrogen; palladium on activated charcoal; In ethanol; for 4h; under 760 Torr;

DOI:10.1021/jo00240a024

upstream raw materials:

N-methoxylamine hydrochloride

vanillin

Downstream raw materials:

vanillylamine hydrochloride