methyl 3-cyclopropylamino-2-(2,4-dichloro-5-fluorobenzoyl)acrylate

Base Information Edit

Chemical Name:methyl 3-cyclopropylamino-2-(2,4-dichloro-5-fluorobenzoyl)acrylate
CAS No.:104600-21-7
Molecular Formula:C₁₄H₁₂Cl₂FNO₃
Molecular Weight:332.159
Hs Code.:
Mol file:104600-21-7.mol

Synonyms:methyl 3-cyclopropylamino-2-(2,4-dichloro-5-fluorobenzoyl)acrylate

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Chemical Property of methyl 3-cyclopropylamino-2-(2,4-dichloro-5-fluorobenzoyl)acrylate Edit

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Technology Process of methyl 3-cyclopropylamino-2-(2,4-dichloro-5-fluorobenzoyl)acrylate

There total 3 articles about methyl 3-cyclopropylamino-2-(2,4-dichloro-5-fluorobenzoyl)acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 90087-77-7
methyl 3-pyrrolidinoacrylate

: 86393-34-2
2,4-dichloro-5-fluorobenzoyl chloride

: methyl 3-(1-pyrrolidinyl)-2-(2,4-dichloro-5-fluorobenzoyl)acrylate

: 104600-21-7
methyl 3-cyclopropylamino-2-(2,4-dichloro-5-fluorobenzoyl)acrylate

Guidance literature:: With triethylamine; In 1,4-dioxane; dichloromethane; water;

Reference yield:

: 704-10-9
2,4-dichloro-5-fluoroacetophenone

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 616-38-6
carbonic acid dimethyl ester

: 77-78-1
dimethyl sulfate

: 765-30-0
Cyclopropylamine

: 104600-21-7
methyl 3-cyclopropylamino-2-(2,4-dichloro-5-fluorobenzoyl)acrylate

Guidance literature:: 2,4-dichloro-5-fluoroacetophenone; carbonic acid dimethyl ester; With sodium hydride; In toluene; at 70 - 80 ℃; for 3h;

N,N-dimethyl-formamide; dimethyl sulfate; In toluene; at 33 - 35 ℃; for 3h;

Cyclopropylamine; In toluene; at 5 - 20 ℃; for 3h; Further stages.;