4-(2',5'-dimethoxy-3',4',6'-trimethylphenyl)-2-methyl-2-butenol

Base Information

• Chemical Name: 4-(2',5'-dimethoxy-3',4',6'-trimethylphenyl)-2-methyl-2-butenol
• CAS No.: 104679-53-0
• Molecular Formula: C₁₆H₂₄O₃
• Molecular Weight: 264.365
• Mol file: 104679-53-0.mol

Synonyms:4-(2',5'-dimethoxy-3',4',6'-trimethylphenyl)-2-methyl-2-butenol

Chemical Property of 4-(2',5'-dimethoxy-3',4',6'-trimethylphenyl)-2-methyl-2-butenol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-(2',5'-dimethoxy-3',4',6'-trimethylphenyl)-2-methyl-2-butenol

There total 2 articles about 4-(2',5'-dimethoxy-3',4',6'-trimethylphenyl)-2-methyl-2-butenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-methyl-3,4-epoxy-1-butene (7437-61-8) + 2,5-dimethoxy-3,4,6-trimethylbenzylmagnesium bromide + lithium tetrachlorocuprate (Li2 CuCl4) → 4-(2',5'-dimethoxy-3',4',6'-trimethylphenyl)-2-methyl-2-butenol (104679-53-0)

Guidance literature:

With ammonium chloride; In tetrahydrofuran;

Reference yield:

4-(2',5'-dihydroxy-3',4',6'-trimethyl-phenyl)-2-methyl-2-butenol (77878-68-3) + tert-butylamine hydrobromide (60469-70-7) + dimethyl sulfate (77-78-1) → 4-(2',5'-dimethoxy-3',4',6'-trimethylphenyl)-2-methyl-2-butenol (104679-53-0)

Guidance literature:

With sodium hydroxide; potassium carbonate; In dichloromethane; water;

Reference yield:

titanium(IV) isopropylate (546-68-9) + tert.-butylhydroperoxide (75-91-2) + 4-(2',5'-dimethoxy-3',4',6'-trimethylphenyl)-2-methyl-2-butenol (104679-53-0) + dibutyl tartrate (344268-32-2,15763-01-6) → (2R,3R)-4-(2',5'-dimethoxy-3',4',6'-trimethylphenyl)-2,3-epoxy-2-methylbutanol (96203-90-6)

Guidance literature:

With sodium hydroxide; In diethyl ether; dichloromethane;

upstream raw materials:

2-methyl-3,4-epoxy-1-butene

4-(2',5'-dihydroxy-3',4',6'-trimethyl-phenyl)-2-methyl-2-butenol

tert-butylamine hydrobromide

dimethyl sulfate

Downstream raw materials:

(2R,3R)-4-(2',5'-dimethoxy-3',4',6'-trimethylphenyl)-2,3-epoxy-2-methylbutanol