methyl 3,5-dibromo-4-(4-methoxy-5-fluoro-3-isopropylphenoxy)phenylacetate

Base Information

Chemical Name:methyl 3,5-dibromo-4-(4-methoxy-5-fluoro-3-isopropylphenoxy)phenylacetate
CAS No.:649725-44-0
Molecular Formula:C₁₉H₁₉Br₂FO₄
Molecular Weight:490.164
Hs Code.:

Synonyms:methyl 3,5-dibromo-4-(4-methoxy-5-fluoro-3-isopropylphenoxy)phenylacetate

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Chemical Property of methyl 3,5-dibromo-4-(4-methoxy-5-fluoro-3-isopropylphenoxy)phenylacetate

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Technology Process of methyl 3,5-dibromo-4-(4-methoxy-5-fluoro-3-isopropylphenoxy)phenylacetate

There total 2 articles about methyl 3,5-dibromo-4-(4-methoxy-5-fluoro-3-isopropylphenoxy)phenylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 649725-42-8
methyl[3,5-dibromo-4-(5-isopropyl-4-methoxy-3-nitrophenoxy)phenyl]acetate

: 649725-44-0
methyl 3,5-dibromo-4-(4-methoxy-5-fluoro-3-isopropylphenoxy)phenylacetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 457 mg / sodium hydrosulfite / ethanol / 48 h / Heating

2.1: nitrosonium tetrafluoroborate / CH₂Cl₂ / 1 h / 0 °C

2.2: 205 mg / o-xylene / 1 h / Heating

With sodium disulfite; nitrosonium tetrafluoroborate; In ethanol; dichloromethane;
DOI:10.1016/j.bmcl.2007.05.049

Reference yield:

: 219692-15-6
(3,5-dibromo-4-(5-isopropyl-4-methoxy-phenoxy)-phenyl)-acetic acid methyl ester

: 649725-44-0
methyl 3,5-dibromo-4-(4-methoxy-5-fluoro-3-isopropylphenoxy)phenylacetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1.1 g / nitric acid / benzene / 1 h / 20 °C

2.1: 457 mg / sodium hydrosulfite / ethanol / 48 h / Heating

3.1: nitrosonium tetrafluoroborate / CH₂Cl₂ / 1 h / 0 °C

3.2: 205 mg / o-xylene / 1 h / Heating

With sodium disulfite; nitric acid; nitrosonium tetrafluoroborate; In ethanol; dichloromethane; benzene;
DOI:10.1016/j.bmcl.2007.05.049

Reference yield: 99.0%

: 649725-44-0
methyl 3,5-dibromo-4-(4-methoxy-5-fluoro-3-isopropylphenoxy)phenylacetate

: 649725-45-1
methyl[3,5-dibromo-4-(3-fluoro-5-isopropyl-4-methoxyphenoxy)phenyl]acetic acid

Guidance literature:: methyl 3,5-dibromo-4-(4-methoxy-5-fluoro-3-isopropylphenoxy)phenylacetate; With lithium hydroxide; In tetrahydrofuran; water; at 20 ℃;

With hydrogenchloride; In tetrahydrofuran; water;