2-{[(1S)-1-methylthio]-ethyl}phenylselenenyl iodide

Base Information

• Chemical Name: 2-{[(1S)-1-methylthio]-ethyl}phenylselenenyl iodide
• CAS No.: 919081-11-1
• Molecular Formula: C₉H₁₁ISSe
• Molecular Weight: 357.117

Synonyms:2-{[(1S)-1-methylthio]-ethyl}phenylselenenyl iodide

Chemical Property of 2-{[(1S)-1-methylthio]-ethyl}phenylselenenyl iodide

Chemical Property:

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Technology Process of 2-{[(1S)-1-methylthio]-ethyl}phenylselenenyl iodide

There total 1 articles about 2-{[(1S)-1-methylthio]-ethyl}phenylselenenyl iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

C9H12SSe2 → 2-{[(1S)-1-methylthio]-ethyl}phenylselenenyl iodide (919081-11-1)

Guidance literature:

With iodine; In tetrachloromethane; diethyl ether; at 0 ℃; for 0.5h;

DOI:10.1002/ejoc.200600517

Reference yield:

2-{[(1S)-1-methylthio]-ethyl}phenylselenenyl iodide (919081-11-1) + styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) → (1R)-2-{2-[(1S)-1-(methylthio)ethyl]phenylselenenyl}-1-phenylethanol (919081-20-2) + (S)-2-[2-((S)-1-Methylsulfanyl-ethyl)-phenylselanyl]-1-phenyl-ethanol

Guidance literature:

With water; In acetonitrile; at -30 ℃; for 72h;

DOI:10.1002/ejoc.200600517

Reference yield:

2-{[(1S)-1-methylthio]-ethyl}phenylselenenyl iodide (919081-11-1) + (E)-3-hexenoic acid (1577-18-0) → (4R,5S)-5-ethyl-4-{2-[(1S)-1-(methylthio)ethyl]phenylselenenyl}-dihydrofuran-2(3H)-one + 5-ethyl-4-({2-[(1S)-1-(methylthio)ethyl]phenyl}seleno)dihydrofuran-2(3H)-one

Guidance literature:

With sodium hydrogencarbonate; In dichloromethane; at 20 ℃; for 72h;

DOI:10.1002/ejoc.200600517

Downstream raw materials:

(1R)-2-{2-[(1S)-1-(methylthio)ethyl]phenylselenenyl}-1-phenylethanol

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